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219 results about "Olive leaf extract" patented technology

Olive leaf extract is a natural source of wellness with therapeutic properties that are: gastroprotective (protects digestive system) neuroprotective (protects central nervous system)

Synsepalum dulcificum Denill tree branch and leaf extract and extraction method and application of extract

The invention relates to an extraction method for a Synsepalum dulcificum Denill tree branch and leaf extract. The extraction method comprises the following steps of: crushing Synsepalum dulcificum Denill tree branches and leaves to obtain an extracted raw material; adding ethanol water; performing reflux extraction for 2-5 hours; filtering; performing reduced pressure distillation on supernate; performing freeze drying to obtain branch and leaf crude extract dry powder; dissolving the branch and leaf crude extract dry powder in water; performing macroporous resin treatment; then, eluting by using the ethanol water to obtain drips; and respectively performing vacuum concentration and the freeze drying to obtain a refined branch and leaf extract. The total phenol content of the obtained extract is 66.5 percent, and the total phenol content of a branch extract is 84.1 percent. The diphenylpicrylphenylhydrazine (DPPH) scavenging activity of the extract is 7.9 and 7.8 times of that of glutathione, and the oxygen radical absorbing capacity of the extract is 7.0 and 6.2 times of that of the glutathione. The extract is good in inhibitory activity on xanthine oxidase and can be used for preparing antioxidants, gout suppressants and health-care products.
Owner:万福群

Anti-tumor traditional Chinese medicinal agent

The invention discloses an anti-tumor traditional Chinese medicinal agent, which is prepared from the following raw materials in parts by weight: 10-20 parts of camptotheca acuminata, 5-10 parts of mockstrawberry lyophilized powder, 5-10 parts of fermented nostoc powder, 2-10 parts of toad, 30-40 parts of herba agrimoniae, 10-15 parts of a milk thistle extract, 10-15 parts of a solanum lyratum extract, 5-10 parts of bark of juglans mandshurica maxim, 10-15 parts of an olive leaf extract, 5-10 parts of a red jujube leaf extract, 5-10 parts of celery powder, 10-15 parts of a beet root extract, 10-15 parts of a blood orange extract, 6-10 parts of spreading hedyotis herb and 15-20 parts of radix stephaniae tetrandrae. The traditional Chinese medicinal agent disclosed by the invention has functions of removing toxins and eliminating stagnation, promoting blood circulation and removing stasis, benefiting qi and nourishing yin, killing and injuring tumor cells, inhibiting growth of cancer cells, controlling disease development and boosting immunity. The medicine, which is generally prepared from natural ingredients, is safe to take and free from obvious side effects; and based upon clinical observation for years, no adverse reaction occurs in patients; therefore, the medicine is suitable for the patients to take for a long time.
Owner:XINXIANG MEDICAL UNIV

Method for preparing high-purity hydroxytyrosol by using high-speed counter-current chromatography and high performance liquid chromatography in combined manner

The invention discloses a method for preparing high-purity hydroxytyrosol by using high-speed counter-current chromatography and high performance liquid chromatography in a combined manner. The method comprises the following steps of performing enzymolysis on an olive leaf extract; extracting with ethyl acetate and concentrating into hydroxytyrosol ointment of which hydroxytyrosol content is 5%-20%; mixing solvents such as petroleum ether, ethyl acetate, methanol and water proportionally; using the mixture as a high-speed counter-current solvent system under the condition that an upper phase is a fixed phase while a lower phase is a mobile phase; dissolving the hydroxytyrosol ointment in the lower phase to obtain a test article; fully filling multilayered coil separating columns of a high-speed counter-current chromatographic instrument in the fixed phase; injecting the mobile phase at revolving speed of 500-1800 r/min and at flowing speed of 1-5mL/min; and detecting by using an ultraviolet detector of which the wave length is 210-280 nanometers. Normal phase centrifugal rotation is implemented in a whole centrifugal process for 30-300 minutes. When the mobile phase begins to flow out of chromatographic columns, distillate is collected, and after the distillate is detected by HPLC (high performance liquid chromatography), the hydroxytyrosol of which the purity is 60-90% can be prepared. The method is easy to operate and low in pollution; and the purity of the separated hydroxytyrosol is high.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Method and apparatus used for preparing olive leaf extract

The invention discloses a method and an apparatus used for preparing an olive leaf extract. The method comprises the steps that: olive leaves are subjected to ultrasonic vacuum boiling extraction by using a mixed solvent; vacuum pump-filtration is carried out, such that a clarified liquid is obtained; fat-soluble impurities are removed through petroleum ether extraction, and a lower-layer clear solution is obtained; the clear solution is subjected to rotary evaporation until no alcohol smell is left in the solvent; the solution is diluted; the diluant is subjected to macroporous resin purification; the obtained solution is subjected to standing for a period of time, such that oleuropein and flavonoid substances are sufficiently absorbed; the oleuropein is eluted by using an ethanol-water mixed solvent with a proper concentration, and a target liquid is collected; the collected target liquid is subjected to dextrane gel purification; standing is carried out, and an ethanol-water solution is used for eluting; a eluant containing effective components is collected; the collected eluant is subjected to rotary evaporation until no alcohol smell is left; and the obtained material is dried, such that the extract is obtained. The oleuropein content of the extract reaches 85-92%, and the total flavonoid content of the extract reaches 25-35%. The method has the advantages of simple operation, short extraction time, high efficiency, high product recovery rate, good quality, and stable quality.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Hydroxytyrosol extraction method high in percent conversion and recovery percent

ActiveCN103709014AHigh yieldOvercome the defect of incomplete hydrolysisOrganic chemistryOrganic compound preparationHydroxytyrosolAcetic acid
The invention discloses a hydroxytyrosol extraction method high in percent conversion and recovery percent. The hydroxytyrosol extraction method comprises the following steps of: 1) obtaining an olive leaf extract and concentrating the extract; 2) adding concentrated hydrochloric acid accounting for 1-2% of the weight of the extract to the obtained extract, increasing the temperature to the range from 85 to 95 DEG C, and preserving heat for hydrolysis for 20-40min; cooling the obtained hydrolysate to the normal temperature and then adding the concentrated hydrochloric acid accounting for 4-8% of the weight of the extract, and hydrolyzing at the normal temperature for 100-150 min to obtain a secondary hydrolysate; 3) regulating the pH value of the secondary hydrolysate to the range from 6.0 to 6.5, extracting with ethyl acetate, recovering the solvent from the extract phase, and drying to obtain the hydroxytyrosol. The hydroxytyrosol extraction method has the advantages that the pattern of intermittent twice hydrolysis is adopted, so that the shortcoming of non-complete once hydrolysis in the prior art is overcome and the percent conversion of decomposing and converting oleuropein into the hydroxytyrosol is effectively increased to be above 98.5%, and in the mean time, the yield of the hydroxytyrosol is increased to be above 95%, and moreover, the process is simplified.
Owner:GUILIN NATURAL INGREDIENTS CORP

Hair loss preventive shampoo and method for manufacturing same

The invention provides hair loss preventive shampoo. The hair loss preventive shampoo comprises Chinese herbal medicine extract and shampoo base materials. The Chinese herbal medicine extract comprises 20-30 parts of polygonum multiflorum extract, 8-15 parts of barbary wolfberry fruit extract, 10-15 parts of black sesame extract, 10-15 parts of olive leaf extract, 10-20 parts of green tea extract, 10-15 parts of dried ginger, 10-18 parts of litsea glutinosa root extract, 12-18 parts of aloe extract, 6-12 parts of common club moss herb, 6-12 parts of lotus seed extract, 5-8 parts of safflower extract, 5-8 parts of folium artemisiae argyi extract, 2-10 parts of herba leonuri extract, 1-8 parts of prunella vulgaris extract and 1-5 parts of angelica sinensis extract which are mixed with one another to obtain the Chinese herbal medicine extract; the shampoo base materials comprise 40-50 parts of sodium dodecyl sulfate, 40-60 parts of water, 5-10 parts of cocamides, 2-4 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 0.4-0.6 part of essence and 0.05-0.1 part of preservatives. The invention further provides a method for manufacturing the hair loss preventive shampoo. The hair loss preventive shampoo and the method have the advantages that hair loss can be reduced by the hair loss preventive shampoo manufactured by the aid of the method, the blood circulation of the scalp of users can be promoted, the hair of the users can be effectively protected and moistened, and dirt in the scalp of the users can be effectively removed.
Owner:农杰
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