Particulate mixtures, kits, inks, methods and articles of manufacture
A technology of mixtures and granules, which is applied in the fields of granule mixtures, cartridges, inks, and products, and can solve problems such as inappropriate application and high viscosity
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[0151] The invention will now be further described with reference to the following examples, which are illustrative and not limiting of the invention.
[0152] Preparation of glass frit particles
[0153] Commercially available frits (i), (ii) and (iii) were obtained from Johnson Matthey. Glass frit (i) (Johnson Matthey Product No. 5466) is a lead-free, boron-free bismuth-silicate glass frit having a silica content of approximately 15% by weight. Glass frit (ii) (Johnson Matthey Product No. 5317) is a lead-free bismuth-based glass frit comprising approximately 13 wt% boron oxide and less than 5 wt% silica. The frit (iii) is a bismuth silicate frit (Johnson Matthey Product No. 5405) comprising greater than 5 wt% silica and greater than 5 wt% boron oxide.
[0154] The glass frits (i), (ii) and (iii) were then each subjected to jet milling to obtain coarse glass frit particles with a D90 particle size of about 5.5 μm. This coarse frit particles were then subjected to wet bea...
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