Preparation method of polycarboxylic acid admixture for reducing viscosity of concrete
A technology of polycarboxylic acid and admixture, which is applied in the field of preparation of polycarboxylic acid admixture, can solve the problems of increasing the viscosity of fresh concrete and reducing the concrete water-cement ratio, and achieve the effect of reducing viscosity and solving contradictions
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[0028]Such asfigure 1As shown, the preparation method of the polycarboxylic acid admixture for reducing the viscosity of concrete in the embodiment of the present invention includes the following steps:
[0029]In step 11, the cyclic polyether and deionized water are configured into an intermediate solution, and the temperature of the intermediate solution is maintained at a preset first temperature.
[0030]In the technical scheme of the present invention, a variety of cyclic polyethers can be used to prepare the above-mentioned intermediate solution.
[0031]For example, as an example, in a preferred embodiment of the present invention, the molecular weight of the cyclic polyether is 1500-2700.
[0032]For another example, as an example, in a preferred embodiment of the present invention, the cyclic polyether is an itaconate type cyclic polyether.
[0033]For another example, as an example, in another preferred embodiment of the present invention, the itaconate cyclic polyether is a substance ha...
specific Embodiment 1
[0059]Dissolve 60 parts of cyclic polyether (molecular weight 1500) in 80 parts of deionized water, stir evenly until completely dissolved, prepare an intermediate solution, and heat the intermediate solution to 60°C and maintain the temperature; then, add 15.2 Acrylic acid, 0.7 part ammonium persulfate, 0.1 part mercaptopropionic acid were added and dissolved in 30 parts of water to form a solution as a dropping liquid; in 2.5 hours, the dropping liquid was added uniformly while stirring In the intermediate solution in the reaction kettle; after the dripping is completed, keep the temperature of the solution at 60° C., and then stir for 1.5 hours to complete, to obtain the polycarboxylic acid admixture.
specific Embodiment 2
[0061]Dissolve 60 parts of cyclic polyether (molecular weight 2000) in 100 parts of deionized water, stir evenly to completely dissolve, prepare an intermediate solution, and heat the intermediate solution to 70°C and maintain the temperature; then, add 7.2 Acrylic acid, 0.5 part ammonium persulfate, 0.15 part mercaptopropionic acid were added and dissolved in 30 parts of water to form a solution as a dripping liquid; in 1.5 hours, while stirring, the dripping liquid was added uniformly In the intermediate solution in the reaction kettle; after the dripping is completed, keep the temperature of the solution at 70°C, and then stir for 1.5 hours to complete, to obtain the polycarboxylic acid admixture.
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