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A Heat Treatment Method for Laser Selective Melting and Forming Nickel-based Superalloy

A nickel-based superalloy, laser selective melting technology, used in heat treatment furnaces, heat treatment equipment, furnaces, etc., can solve the problem of mechanical properties not meeting the development needs, etc., to weaken the growth tendency, improve low-temperature plasticity, toughness, fine The effect of grain size

Active Publication Date: 2022-04-08
XIAN SPACE ENGINE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The technical problem solved by the present invention is: aiming at the problem that the mechanical performance index after heat treatment in the prior art does not meet the development requirements, a heat treatment method for forming nickel-based superalloys by laser selective melting is provided. -3 In a vacuum environment of Pa, raise the temperature from room temperature to 900°C±10°C and keep it for 0.5h, then raise the temperature to 1050°C~1100°C and keep it for 1h~4h, then inflate and cool; -3 Pa vacuum environment, temperature at 735 ° C ± 15 ° C under the condition of heat preservation for 8h ~ 10h, inflated to cool

Method used

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  • A Heat Treatment Method for Laser Selective Melting and Forming Nickel-based Superalloy
  • A Heat Treatment Method for Laser Selective Melting and Forming Nickel-based Superalloy

Examples

Experimental program
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Effect test

Embodiment 1

[0030] Take a certain type of engine turbo pump centrifugal wheel as an example.

[0031] (1) The workpiece is made of nickel-based superalloy by laser selective melting.

[0032] (2) Heat treatment: the centrifugal wheel after separating the substrate is heat treated in a vacuum heat treatment furnace. The pressure in the furnace is not more than 10 -3 Pa, after the environment in the furnace meets the requirements, raise the temperature from room temperature to 900°C for 0.5h, then raise the temperature to 1065°C for 4h, after the heat preservation is completed, backfill with argon to cool, and the pressure of backfill with argon is 3.0×10 5 Pa, immediately start the stirring fan in the equipment, cool to below 80°C and leave the furnace for air cooling; then heat treatment in a vacuum heat treatment furnace, the pressure in the furnace is not greater than 10 -3 Pa, after the environment in the furnace meets the requirements, heat it up to 735°C and keep it warm for 10 hou...

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Abstract

The invention discloses a heat treatment method for a nickel-based superalloy formed by selective laser melting, which includes: ‑ 3 In a vacuum environment of Pa, raise the temperature from room temperature to 900℃±10℃ and keep it for 0.5h, then raise the temperature to 1050℃~1100℃ and keep it for 1h~4h, then inflate and cool; ‑3 Pa vacuum environment, temperature at 735 ° C ± 15 ° C under the condition of heat preservation for 8h ~ 10h, air cooling. By controlling the grain size of the austenite matrix and the type and quantity of precipitated phases, the low-temperature plasticity and toughness are improved, and the application range of the material is expanded. ‑196℃, Rm not less than 1500N / mm 2 , Rp0.2 not less than 1100N / mm 2 , A not less than 12%, Z not less than 20%, KU2 not less than 60J.

Description

[0001] technology field [0002] The invention relates to the technical field of metal additive manufacturing, in particular to a heat treatment method for laser selective melting and forming of a nickel-based superalloy. Background technique [0003] The nickel-based superalloy involved in the present invention is a Ni-Cr-Fe-based precipitation-hardening superalloy with a long-term service temperature range of -253°C to 650°C, excellent comprehensive mechanical properties, good processing performance and welding performance. Alloys have good mechanical properties and structural stability in low-temperature media (such as liquid oxygen or liquid hydrogen, etc.), and are widely used in liquid oxygen methane engines, liquid hydrogen and liquid oxygen engines and other liquid rocket engines that use cryogenic propellants. Components such as turbo pump housings, centrifugal wheels, etc. [0004] Laser selective melting forming technology has the characteristics of high manufactur...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22F1/02C22F1/10B22F10/64C21D9/32B33Y40/20
CPCC22F1/02C22F1/10B22F3/24C21D9/32B33Y40/20B22F2003/248
Inventor 同立军杨欢庆雷钥郑伟白瑞兴王丁雯秦川
Owner XIAN SPACE ENGINE CO LTD
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