Convenient-to-clean water-absorbing color-changing cat litter and preparation method thereof
A technology of cat litter and color-changing silica gel, applied in chemical instruments and methods, manufacturing tools, wood treatment, etc., can solve the problems of large dust, bad for cat health, and easy to get stuck.
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Embodiment 1
[0034]The specific preparation process of modified bentonite is as follows:
[0035] Step S1, weigh 34.5g of sodium hydroxide into a flask, add 100mL of distilled water and stir to mix, after the sodium hydroxide is dissolved, add 55g of bentonite and continue ultrasonic oscillation for 30 minutes, then transfer to an ice-water bath, and use a constant pressure dropping funnel Add 12g of acrylic acid dropwise to the flask at a rate of 2 drops / second to prepare a mixed solution for subsequent use;
[0036] Step S2, add 0.55g of monoglyceride stearate and 35mL of cyclohexane into the flask, under the condition of blowing nitrogen, heat until the dispersant is dissolved, then add the mixed solution prepared in step S1, 0.6g of benzoyl peroxide And 1.1g1,3-propanediol, after stirring and reacting for 3 hours, cyclohexane was removed by distillation under reduced pressure to obtain the product;
[0037] Step S3, put the product prepared in step S2 into a vacuum oven, dry it under ...
Embodiment 2
[0049] The specific preparation process of modified bentonite is as follows:
[0050] Step S1, weigh 38g of sodium hydroxide and put it into a flask, add 110mL of distilled water to stir and mix, after the sodium hydroxide is dissolved, add 50g of bentonite and continue ultrasonic oscillation for 35 minutes, then transfer to an ice-water bath, and use a constant pressure dropping funnel to Add 13g of acrylic acid dropwise in the flask at a rate of 1 drop / second to prepare a mixed solution for subsequent use;
[0051] Step S2, add 0.6g of monoglyceride stearate and 40mL of cyclohexane into the flask, under nitrogen, heat until the dispersant dissolves, then add the mixed solution prepared in step S1, 0.7g of benzoyl peroxide And 1.2g1,3-propanediol, after stirring and reacting for 2 hours, the cyclohexane was removed by distillation under reduced pressure to obtain the product;
[0052] Step S3, put the product prepared in step S2 into a vacuum oven, dry it under reduced press...
Embodiment 3
[0064] The specific preparation process of modified bentonite is as follows:
[0065] Step S1, weigh 40g of sodium hydroxide and put it into a flask, add 120mL of distilled water to stir and mix, after the sodium hydroxide is dissolved, add 55g of bentonite and continue ultrasonic oscillation for 40 minutes, then transfer to an ice-water bath, and use a constant pressure dropping funnel to Add 14g of acrylic acid dropwise in the flask at a rate of 3 drops / second to prepare a mixed solution for subsequent use;
[0066] Step S2, add 0.6g of monoglyceride stearate and 35mL of cyclohexane into the flask, under the condition of blowing nitrogen, heat until the dispersant is dissolved, then add the mixed solution prepared in step S1, 0.8g of benzoyl peroxide And 1.2g1,3-propanediol, after stirring and reacting for 3 hours, the cyclohexane was removed by distillation under reduced pressure to obtain the product;
[0067] Step S3, put the product prepared in step S2 into a vacuum ove...
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