Low-viscosity flowing type high-thermal-conductivity flame-retardant packaging material and preparation method thereof

A packaging material, flow-type technology, applied in the direction of adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve the problems of lack of fluidity, poor flame retardant performance, high consistency, and achieve good curing stability. , the effect of good bonding performance

Active Publication Date: 2021-07-09
MIANYANG WELLS ELECTRONICS MATERIAIS
View PDF10 Cites 7 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] One-component flame retardant and thermally conductive packaging materials need to obtain high thermal conductivity and excellent flame retardant performance, usually need to add a large amount of thermally conductive and flame retardant fillers, which will lead to The consistency of the glue is high, the manufacturability is poor, and it does not have any fluidity. In addition, the filling of a large amount of fillers will also make the adhesive performance of the glue poor; while the filling of low fillers can make the glue fluid, but It will also lead to the problem that the thermal conductivity of the glue is greatly reduced and the flame retardant performance is deteriorated.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Low-viscosity flowing type high-thermal-conductivity flame-retardant packaging material and preparation method thereof
  • Low-viscosity flowing type high-thermal-conductivity flame-retardant packaging material and preparation method thereof
  • Low-viscosity flowing type high-thermal-conductivity flame-retardant packaging material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] (1) React 1.5 parts of γ-aminopropyltriethoxysilane with γ-glycidyloxypropyltrimethoxysilane (molar ratio is 1:2), 3.5 parts of methyltrimethoxysilane and 1.9 parts of acetyl The ethyl acetate titanium complex was pre-mixed uniformly in a clean and airtight container, and then the mixture was reacted at 45 degrees for 90 minutes.

[0060] (2) Add 632 parts of the above-mentioned 1# base glue and 20 parts of the above-mentioned bistrimethoxy-terminated polysiloxane with a viscosity of 1020 mPa.s into the planetary stirring tank, and stir for 30 minutes at a speed of 40 r / min.

[0061] (3) Add 3.5 parts of fumed silica with a specific surface area of ​​150m2 / g and surface treated with silazane, and stir for 30 minutes at a speed of 45r / min.

[0062] (4) Add 7.7 parts of the mixed reactants in the above-mentioned first step (1), 0.7 parts of divinyltetramethyldisiloxane platinum complex with a platinum content of 3000ppm, and depressurize the planetary stirring tank to -0....

Embodiment 2

[0065] (1) With embodiment 1.

[0066] (2) Add 632 parts of the above-mentioned 2# base glue and 20 parts of the above-mentioned bistrimethoxy-terminated polysiloxane with a viscosity of 1020 mPa.s into the planetary stirring tank, and stir for 30 minutes at a speed of 40 r / min.

[0067] (3) Add 2.5 parts of fumed silica with a specific surface area of ​​150m2 / g and surface treated with silazane, and stir for 30 minutes at a speed of 45r / min.

[0068] (4) (5) with embodiment 1.

Embodiment 3

[0070] (1) Same as embodiment 1

[0071] (2) Add 627 parts of the above-mentioned 4# base glue and 20 parts of the above-mentioned bistrimethoxy-terminated polysiloxane with a viscosity of 1020 mPa.s into the planetary stirring tank, and stir for 30 minutes at a speed of 40 r / min.

[0072] ⑶Add 3.5 parts specific surface area 150m 2 / g, fumed silica whose surface was treated with silazane, stirred at 45r / min for 30 minutes.

[0073] (4) (5) with embodiment 1.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
specific surface areaaaaaaaaaaa
specific surface areaaaaaaaaaaa
Login to view more

Abstract

The invention discloses a low-viscosity flowing type high-thermal-conductivity flame-retardant packaging material and a preparation method thereof. The packaging material comprises the following components in parts by mass: 70-100 parts of alkoxy-terminated polysiloxane; 0-30 parts of dimethyl silicone oil; 400-700 parts of a functional filler; 0.5-10 parts of a surface treating agent; 1-10 parts of an anti-settling agent; 0.5-5 parts of a cross-linking agent; 0.5-3 parts of a flame retardant aid; 0.2-2.0 parts of an adhesion promoter; and 1.0-5.0 parts of catalyst. Meanwhile, the invention also provides the preparation method of the low-viscosity flow type high-thermal-conductivity flame-retardant packaging material. The packaging material has relatively low viscosity, good fluidity, a heat conductivity coefficient of 1.5 W / m.K or above and flame retardant property of UL94V0 level, and also has good adhesive property.

Description

technical field [0001] The invention relates to the field of silicone rubber, in particular to a low-viscosity flow type high thermal conductivity flame-retardant packaging material and a preparation method thereof. Background technique [0002] One-component thermally conductive adhesive packaging materials have been widely used in various fields such as aerospace, power equipment, power devices, automotive electronics, and military equipment. They play the role of thermally conductive adhesive and insulation protection, and are a good thermally conductive package Materials, with the increase in power handling of power devices and the trend toward smaller, higher-density electronic modules, the need for heat control is also increasing. At the same time, the structural design of these power devices and electronic modules is becoming more and more Diversification, more and more applications usually require thermally conductive adhesives to have better fluidity to meet the hea...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C09J183/04C09J11/04C09J11/06
CPCC09J183/04C09J11/04C09J11/06C08L2201/02C08K2201/003C08K2003/2227C08K2003/2296C08L83/04C08K13/06C08K9/06C08K7/18C08K3/22C08K5/544C08K5/5419C08K5/5425C08K7/26C08K3/36
Inventor 芦成陆南平赵元刚钟思伟
Owner MIANYANG WELLS ELECTRONICS MATERIAIS
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products