Ginger extract fiber and preparation method thereof
A technology of ginger extract and plant extract, applied in the field of fiber, can solve the problems of old color, affecting the quality of yarn and fabric, poor functional durability, etc., and achieves enhanced lateral binding force, reduced generation of microfibers, and antibacterial effect. lasting effect
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Embodiment 1
[0055] Embodiment 1 A kind of ginger extract fiber and preparation method thereof, comprises the following steps:
[0056] 1. Preparation of cellulose lysate
[0057] 1. Swelling of cellulose pulp
[0058] Immerse the cotton pulp in deionized water and stir ultrasonically for 15 minutes to fully swell the cellulose and reduce the ash content in the pulp.
[0059] 2. Enzyme hydrolysis
[0060] Dehydrate the swollen cotton pulp to a water content of 13%, put it into a reaction kettle, add cellulase solution and buffer solution, adjust the pH to 5, stir at 50°C for 4 hours, and the stirring speed is 200r / min. After stirring, the enzyme is killed at high temperature. Cellulose was obtained after filtering and drying at 80°C for 2.5 hours;
[0061] The ratio of the cellulase solution to the pulp is 25:1; the cellulase content in the cellulase hydrolysis solution is 6%;
[0062] The buffer is 0.1 mol / L phosphate buffer and 0.15 mol / L sodium citrate buffer, the ratio of the two i...
Embodiment 2
[0082] Embodiment 2 A kind of ginger extract fiber and preparation method thereof
[0083] The difference between this embodiment and Example 1 is that the preparation steps of the cellulose dissolving solution are different, and the rest are consistent with Example 1, specifically as follows:
[0084] 1. Swelling of cellulose pulp
[0085] Immerse the bamboo pulp in deionized water and stir it ultrasonically for 13 minutes to fully swell the cellulose and reduce the ash content in the pulp.
[0086] 2. Enzyme hydrolysis
[0087] Dehydrate the swollen bamboo pulp to a water content of 15%, put it into a reaction kettle, add cellulase solution and buffer, adjust the pH to 5.5, stir at 45°C for 3.5h, and the stirring speed is 150r / min, and then inactivate the enzyme at high temperature after stirring , filtered and dried at 85°C for 2 hours to obtain cellulose;
[0088] The ratio of the cellulase solution to the pulp is 20:1; the cellulase content in the cellulase hydrolysis ...
Embodiment 3
[0095] Embodiment 3 A kind of ginger extract fiber and preparation method thereof
[0096] The difference between this embodiment and embodiments 1 and 2 is that the preparation steps of the cellulose dissolving solution are different, and the rest are consistent with embodiments 1 and 2, specifically as follows:
[0097] 1. Swelling of cellulose pulp
[0098]Immerse the wood pulp in deionized water and stir ultrasonically for 18 minutes to fully swell the cellulose and reduce the ash content in the pulp.
[0099] 2. Enzyme hydrolysis
[0100] Dehydrate the swollen wood pulp to a water content of 10%, put it into a reaction kettle, add cellulase solution and buffer solution, adjust the pH to 4.5, stir at 50°C for 3 hours, and the stirring rate is 250r / min, and then inactivate the enzyme at high temperature after stirring. Cellulose was obtained after filtering and drying at 75°C for 3 hours;
[0101] The ratio of the cellulase solution to the pulp is 25:1; the cellulase con...
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