Catalysed membrane
An electrocatalyst and ion-conducting membrane technology, applied in the field of catalytic ion-conducting membranes, can solve the problems of not showing high performance, low permeability, etc.
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[0115] Preparation of layer A ink
[0116] Layer A ink was made by mixing 2 g of carbon powder with 7.07 g of aqueous Solvay 830EW ionomer solution (Aquivion, 25% by weight) using a spatula to ensure complete wetting of the carbon powder. 2.85 g of pure propan-1-ol and 4.82 g of water were added to the mixture to achieve a 22% by weight propan-1-ol / water ratio in the solvent mixture and stirred well. The ionomer content in the carbon ink was 90% by weight relative to the weight of carbon. in a 5mm diameter with ten Beads Speedmixer TM Process the mixture in a DAC 150FVZ-K until optimum grain breakdown is achieved. Stop the ink treatment and stir after 5 minutes to avoid overheating of the ink during treatment.
[0117] Two different Layer A inks were prepared, each ink containing a different carbon. As described in WO2013 / 045894, the layer A1 (LA1) ink contains carbon specifically designed for use in fuel cells. Layer A2 (LA2) ink contained Ketjen EC-300J.
[0118] ...
Embodiment 5
[0182] Example 5 corresponds to Comparative Example 3, with layer A added. The performance of Example 5 in air at high current density is better than that of Comparative Example 3 and close to that of Comparative Example 5. The permeability of the electrocatalyst layer in embodiment 5 is 17nm 2 . Therefore, layer A has improved performance in air at high current densities for electrocatalyst layers with high kinetic performance.
Embodiment 6
[0183] Example 6 corresponds to Comparative Example 4, with layer A added. The performance of Example 6 in air at high current density is similar to that of Comparative Example 4. The permeability of the electrocatalyst layer in embodiment 6 is 21nm 2 . Table 8 summarizes the permeability of the layers in these examples.
[0184] Table 8
[0185] Permeability nm 2
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