An antigen-binding molecule, a pharmaceutical composition, and a method
A technology of antigen-binding molecules and binding capabilities, applied in the fields of botanical equipment and methods, biochemical equipment and methods, chemical instruments and methods, etc.
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Embodiment 1
[0654] Preparation of recombinant C1r2s2
[0655] 1.1. Expression and purification of cynomolgus monkey C1r2s2 His / Flag tetramer
[0656] Sequences used for expression and purification were: Cynomolgus Cls (SEQ ID NO: 1 ) with a C-terminal GGGGS linker and FLAG tag and Cynomolgus Clr with a C-terminal GGGGS linker and 8×histidine tag. The cynomolgus Clr sequence has the R463QS654A mutation (SEQ ID NO: 2). To express recombinant cynomolgus C1r2s2 His / Flag tetramer, FreeStyle293-F cell line (Thermo Fisher, Carlsbad, CA, USA) was used to transiently co-express cynomolgus C1s-Flag and cynomolgus C1r-His. Conditioned medium expressing recombinant cynomolgus C1r2s2 His / Flag tetramer was applied to anti-FlagM2 affinity resin (Sigma) and eluted with Flag peptide (Sigma). Fractions containing recombinant cynomolgus C1r2s2 His / Flag tetramer were passed through an IMAC column (GE Healthcare) and eluted with an imidazole gradient. The eluted fractions containing the recombinant C1r2s2 ...
Embodiment 2
[0660] 2.1 Preparation of cynomolgus Fcγ receptor (cynomolgus FcγR)
[0661] Synthesis of extracellular domain genes for cynomolgus FcγRs was constructed by cloning the cDNA of each FcγR from cynomolgus monkeys using methods known to those skilled in the art. The amino acid sequence of the constructed FcγR extracellular domain is shown in the sequence list: (for cynomolgus FcγRIa, SEQ ID NO: 5; for cynomolgus FcγRIIa1, SEQ ID NO: 6; for cynomolgus FcγRIIa2, SEQ ID NO: 7; for cynomolgus FcγRIIa3, SEQ ID NO: 8; for cynomolgus FcγRIIb, SEQ ID NO: 9; for cynomolgus FcγRIIIa (R), SEQ ID NO: 10; for cynomolgus FcγRIIIa (S), SEQ ID NO: 11). His-tags were then added to their C-terminals and each of the obtained genes was inserted into expression vectors designed for expression in mammalian cells. The expression vector was introduced into FreeStyle293 cells (Invitrogen) derived from human embryonic kidney cells to express the target protein. After culturing, the resulting culture su...
Embodiment 3
[0663] Preparation of anti-C1s antibody
[0664] 3.1. Production of COS0098pHv1 and preparation of COS0098pHv1-SG1077 and COS0098pHv1-SG1
[0665] The variable regions of some anti-C1s antibodies COS0098bb (VH, SEQ ID NO: 12; VL, SEQ ID NO: 13, as described in PCT / JP2018 / 042054) were humanized to reduce the potential immunogenicity of the antibodies. The complementarity determining regions (CDRs) of the anti-C1s rabbit antibody were grafted onto the cognate human antibody framework (FR) using the conventional CDR grafting method (Nature 321:522-525 (1986)). The gene encoding the humanized VH was synthesized and combined with human IgG1 CH (SG1, SEQ ID NO: 14), modified human IgG1 CH such as SG1077 (SEQ ID NO: 15) and SG1148 (SEQ ID NO: 16). The gene encoding the humanized VL was synthesized and combined with human CL (SK1, SEQ ID NO: 26) and modified human CL (KOMC, SEQ ID NO: 17). Those combined sequences were cloned into expression vectors.
[0666] A number of mutations ...
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