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Cannabis sativa leaf extract as well as preparation method and application thereof

An extract and cannabis leaf technology, applied in the field of cannabis leaf extract and its preparation, can solve the problem of easy repetition of symptoms and other problems, achieve the effects of inhibiting bacteria, maintaining normal oral flora, and high product safety

Active Publication Date: 2022-03-11
云南康恩贝植物研究院有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Because patients with bleeding gums and dental calculus need to experience the cumbersomeness of drug treatment and regular tooth cleaning, and the symptoms are easy to repeat, there is an urgent need to develop a daily care preparation that can effectively prevent and treat such symptoms

Method used

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  • Cannabis sativa leaf extract as well as preparation method and application thereof
  • Cannabis sativa leaf extract as well as preparation method and application thereof
  • Cannabis sativa leaf extract as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] Embodiment 1: Cannabis leaf extract preparation process 1

[0047] A preparation method of cannabis leaf extract, comprising the following steps:

[0048] (1) Pretreatment: the qualified industrial hemp mosaic leaves are pulverized, passed through a 100-mesh sieve, granulated, and dried for later use;

[0049] (2) Subcritical extraction: put 500 kg of industrial hemp mosaic particles in step (1) into a subcritical leaching tank, add the extraction solvent butane, turn on the equipment, the extraction temperature is 80°C, the extraction pressure is 0.8 MPa, and the extraction time is 80°C. 60min, repeated extraction 8 times, separation of medicinal residues, extraction to obtain an oil-soluble mixture; put the obtained oil-soluble mixture into the evaporation system, condense with a compressor and circulating water, recover and recycle the extraction solvent, and obtain 150kg of subcritical extract;

[0050] (3) Subcritical extract is turned to dissolve: to the subcriti...

Embodiment 2

[0054] Embodiment 2: Cannabis leaf extract preparation process 2

[0055] A preparation method of cannabis leaf extract, comprising the following steps:

[0056] (1) Pretreatment: the qualified industrial hemp mosaic leaves are pulverized, passed through a 40-mesh sieve, granulated, and dried for later use;

[0057] (2) Subcritical extraction: put 500 kg of industrial hemp mosaic granules in step (1) into a subcritical leaching tank, add the extraction solvent propane, start the equipment, the extraction temperature is 50°C, the extraction pressure is 0.9 MPa, and the extraction time is 30min, repeated extraction 3 times, separated medicinal residues, extracted to obtain an oil-soluble mixture; put the obtained oil-soluble mixture into the evaporation system, condensed with a compressor and circulating water, recovered and recycled the extraction solvent, and obtained 154kg of subcritical extract;

[0058] (3) Subcritical medicinal extract transfer: to the medicinal extract i...

Embodiment 3

[0062] Embodiment 3: Cannabis leaf extract preparation process 3

[0063] A preparation method of cannabis leaf extract, comprising the following steps:

[0064] (1) Pretreatment: the qualified industrial hemp mosaic leaves are pulverized, passed through an 80-mesh sieve, granulated, and dried for later use;

[0065] (2) Subcritical extraction: put 500 kg of industrial hemp mosaic granules in step (1) into a subcritical leaching tank, add the extraction solvent dimethyl ether, turn on the equipment, the extraction temperature is 25°C, the extraction pressure is 0.18MPa, and the extraction The time is 90 minutes, repeated extraction 5 times, separating the medicinal residue, and extracting to obtain an oil-soluble mixture; put the obtained oil-soluble mixture into the evaporation system, condense with a compressor and circulating water, and recover and recycle the extraction solvent to obtain 141kg of subcritical extract ;

[0066] (3) Subcritical extract is turned to dissolv...

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Abstract

The invention discloses a cannabis sativa leaf extract as well as a preparation method and application thereof. The cannabis sativa leaf extract contains 0.30-0.93 g / g of cannabidiol and 0.05-0.08 mg / g of tetrahydrocannabinol. Wherein cannabidiol is a main medicinal component for inhibiting gingival bleeding and dental calculus; the content of tetrahydrocannabinol is far lower than the content standard of 0.3% (w / w), and the product is safe and free of addiction. The cannabis sativa leaf extract has the effects of inhibiting gingival bleeding and dental calculus, and particularly, after the cannabis sativa leaf extract and the ginkgo leaf extract form the oral care composition, the combination advantage is reflected, the dosage is reduced, and the curative effect is improved. The toothpaste prepared from the oral composition can better improve the healthy environment of teeth and gingiva, consolidate the gingiva structure and effectively treat gingival bleeding and dental calculus, is free of preservatives, is a pure natural, green, safe and effective toothpaste product, and has market popularization prospects.

Description

technical field [0001] The invention relates to a natural plant extract, in particular to a cannabis leaf extract and its preparation method and application. Background technique [0002] Dental calculus is a calcified and partially calcified substance attached to the surface of the teeth. It is an important pathogenic factor in the development of periodontal disease. The clinical manifestations are gingival recession, gingival bleeding, bad breath, and loose teeth. Gingival inflammation refers to acute and chronic inflammation that occurs in gingival tissue. The clinical manifestations are gingival bleeding, redness, swelling, and pain. It continues to develop and invade hard tissues, resulting in periodontitis, including inflammation of gingival tissue and a manifestation of systemic diseases in the gingiva. Bleeding gums are often the main subjective symptoms of gingivitis patients. They often occur when brushing teeth or biting hard objects, and occasionally there may be...

Claims

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Application Information

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IPC IPC(8): A61K36/60A61P1/02A61P7/04A61K8/9789A61K8/9771A61Q11/00A23L33/105
CPCA61K36/60A61K36/16A61P1/02A61P7/04A61K8/9789A61K8/9771A61Q11/00A23L33/105A61K2236/37A61K2236/55A61K2800/592A23V2002/00A61K2300/00A23V2200/312A23V2250/21A23V2250/2122
Inventor 叶洪洋洋陈君平夏婷陈岑刘华春王开锦罗庆辉朱吉乔洪翔
Owner 云南康恩贝植物研究院有限公司
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