Method of recycline fine powder of cracking catalyst
A cracking catalyst and catalyst technology, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, catalyst regeneration/reactivation, etc., can solve problems such as increasing the solid content of oil slurry, economic losses in refineries, and reducing product quality, etc., to achieve Environmental protection, low operating costs, and economical recycling effects
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Embodiment 1
[0019] This example shows that after the catalyst fine powder is treated by the method provided by the present invention, the properties of the obtained catalyst are basically equivalent to those of catalyst products with qualified particle size.
[0020] The test procedure is as follows: the catalyst fine powder less than 20 μm is configured into a slurry with a solid content of 20% by weight, ground with a sand mill, and the feed space velocity is 6h -1 After 5 minutes, the average particle size of the particles in the slurry was 1.2 μm, and the slurry showed good gel properties. The above slurry was directly added to the aged colloid of the original brand of catalyst A with a mixing ratio of 1:1, stirred evenly and then spray-dried to obtain catalyst product B. Catalysts A and B were subjected to hydrothermal aging and test evaluation under the same conditions, and the test results obtained are shown in Table 1.
[0021] catalyst
Embodiment 2
[0023] This example shows that after the catalyst fine powder is treated by the method provided by the present invention, the properties of the obtained catalyst are basically equivalent to those of catalyst products with qualified particle size.
[0024] The test procedure is as follows: the catalyst fine powder is configured into a slurry with a solid content of 50% by weight, ground with a sand mill, and the feed space velocity is 4h -1 After 9 minutes, the average particle size of the particles in the slurry was 1.1 μm, and the slurry showed good gel properties. The above-mentioned slurry was directly added to the aged colloid of the original brand of catalyst A in an amount of 30% by weight, stirred evenly and then spray-dried to obtain catalyst product C. The two catalysts A and C were subjected to hydrothermal aging and test evaluation under the same conditions, and the test results obtained are shown in Table 2.
[0025] catalyst
Embodiment 3
[0027] This example shows that after the catalyst fine powder is treated by the method provided by the present invention, the properties of the obtained catalyst are basically equivalent to those of catalyst products with qualified particle size.
[0028] The test procedure is as follows: the catalyst fine powder is configured into a slurry with a solid content of 40% by weight, ground with a sand mill, and the feed space velocity is 8h -1 After 5 minutes, the average particle size of the particles in the slurry was 1.0 μm, and the slurry showed good gel properties. Send the above slurry to a spray drying device for drying to obtain catalyst D. Catalyst D is mixed with catalyst A, and the weight ratio of mixing is A:D=3:2, and the new catalyst obtained after mixing is E. The two catalysts A and E were subjected to hydrothermal aging and test evaluation under the same conditions, and the test results obtained are shown in Table 3.
[0029] catalyst
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