Process for preparing proton exchange film fuel cell multi component catalyst
A technology of proton exchange membrane and fuel cell, which is applied in the direction of catalyst carrier, chemical instrument and method, physical/chemical process catalyst, etc. It can solve the problems of high cost, lack of resources, and limitation of the practical speed of fuel cell, so as to achieve less reunion, High purity, effect of improving anti-CO poisoning ability
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example 1
[0022] 1) 20 parts of activated carbon, 30 parts of chloroplatinic acid, 30 parts of ruthenium trichloride, and 20 parts of cerium oxide are added to a closed container filled with 75% deionized water to form a premix;
[0023] 2) After the premix is reacted for 6 hours in a nitrogen atmosphere at 200°C and a pressure of 2.5Mpa, it is cooled to room temperature;
[0024] 3) Add 2 parts of sodium thiosulfate and treat at 140°C for 4 hours to uniformly fix platinum, ruthenium and cerium on the original position of the reduction reaction;
[0025] 4) The slurry formed above is filtered, washed, and dried to obtain a PtRuCe / C multi-element catalyst.
example 2
[0027] 1) 25 parts of carbon nanotubes, 50 parts of platinum chloride, 10 parts of ruthenium oxide, and 15 parts of samarium oxide are added to a closed container to which 80% deionized water has been added to form a premix;
[0028] 2) After the premix is reacted for 8 hours at 150°C and a pressure of 2Mpa in an argon atmosphere, it is cooled to room temperature;
[0029] 3) Add 4 parts of sodium dithionite and treat at 120°C for 6 hours to uniformly fix platinum, ruthenium and samarium on the original position of the reduction reaction;
[0030] 4) The slurry formed above is filtered, washed, and dried to obtain a PtRuSm / C multi-element catalyst.
example 3
[0032] 1) 20 parts of activated carbon, 25 parts of platinum oxide, 25 parts of ruthenium oxide, and 30 parts of yttrium oxide are added to a closed container to which 80% deionized water has been added to form a premix;
[0033] 2) After the premix is reacted for 6 hours at 300°C under a pressure of 2Mpa in a nitrogen atmosphere, it is cooled to room temperature;
[0034] 3) Add 2 parts of sodium formate and treat at 200°C for 2 hours to uniformly fix platinum, ruthenium and yttrium on the original position of the reduction reaction;
[0035] 4) The slurry formed above is filtered, washed, and dried to obtain a PtRuY / C multi-element catalyst.
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