Spray agent of dried powder in use for treating hemorrhoid and preparation method
A spray and dry powder technology, applied in pharmaceutical formulations, powder delivery, drug combination and other directions, can solve problems such as inconvenience and inconvenience, and achieve stable and reliable products.
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Embodiment 1
[0016] Embodiment 1, the preparation of Yunnan Baiyao dry powder spray:
[0017] 1. Separation of active ingredients of Yunnan Baiyao:
[0018] Take 1 kg of Yunnan Baiyao powder, extract with 70% ethanol 8, 6, and 6 times heat reflux for 1 hour three times, combine the extracts, concentrate to 50% amount, decolorize with 0.1% solution amount of activated carbon, short (10cm) The silica gel column was used to remove impurities once, concentrated to 20% of the amount, placed overnight at 5-10°C, filtered by ultrafiltration, concentrated in vacuo to dryness, and about 70 g of effective antibacterial, hemostatic and anti-inflammatory parts of Yunnan Baiyao can be obtained (yield ~ 7%).
[0019] 2. Preparation of ultrafine powder of Yunnan Baiyao extract:
[0020] Under the condition of grade 10,000, add 50 g of the antibacterial, hemostatic and anti-inflammatory effective part of Yunnan Baiyao extracted above to 250 g of excipient chitin, grind and mix well, and carry out airflow...
Embodiment 2
[0023] Embodiment 2, the preparation of Yunnan red medicine dry powder spray
[0024] 1. Separation of active ingredients of Yunnan red medicine:
[0025] Get 1 kg of Yunnan Hongyao powder, extract with 70% ethanol 8, 6, 6 times heat reflux for 1 hour three times, combine the extracts, concentrate to 50% amount, decolorize with 0.1% active carbon of solution amount, short (10cm ) silica gel column to remove impurities once, concentrated to 20% of the amount, placed overnight at 5~10°C, filtered by ultrafiltration, concentrated to dryness in vacuum, and about 58g of effective antibacterial, hemostatic and anti-inflammatory parts of Yunnan red medicine can be obtained (yield ~ 5.8%) ).
[0026] 2. Preparation of ultrafine powder of Yunnan red medicine extract:
[0027] Under the condition of 10,000 grades, 50g of the effective part of Yunnan red medicine for antibacterial, hemostatic and anti-inflammation extracted above was added with 100g of polyacrylic acid carbomer (CP), 1...
Embodiment 3
[0030] Embodiment 3, the preparation of compound artemisia annua dry powder spray
[0031] 1. Extraction of effective parts of compound Artemisia annua:
[0032] Take 1 kg of compound Artemisia annua, powder it, extract it three times with 70% ethanol at 8, 6, and 6 times heat reflux for 1 hour, combine the extracts, concentrate to 50%, decolorize with 0.1% solution of activated carbon, short (10cm) silica gel column to remove impurities once, concentrate to 20% amount, place overnight at 5~10°C, filter by ultrafiltration, and concentrate to dryness in vacuum, about 53g of effective parts of Yunnan red medicine for antibacterial, hemostatic and anti-inflammatory can be obtained (yield ~ 5.3%).
[0033] 2. Preparation of superfine powder of compound Artemisia annua extract:
[0034] Under the condition of 10,000 grades, add 50 g of the effective part of the above-mentioned extract of compound Artemisia annua antibacterial, hemostatic and anti-inflammatory to 70 g of hypromell...
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