Polymeric emulsions for ink jet inks
A technology of inkjet ink and polymer, applied in the field of inkjet ink, can solve the problem of increasing the maintenance of printing head, limiting the speed and accuracy of printing operation, affecting the rheology of inkjet ink, etc.
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Embodiment approach
[0036] Procedure for Determination of Slurry Fraction of Acid Monomer Derived Material
[0037] 1. Sample Preparation
[0038] 17.5 g of latex was diluted to 35 g with deionized water and centrifuged at 18,500 rpm for 2 hours at 4°C in a DuPontSorvall Super T-21 centrifuge equipped with an SL-50T rotor. After centrifugation, the clear supernatant was carefully decanted. Dilute 17.5 g of the supernatant to 30 g with deionized water.
[0039] 2. Titrate 30 grams of sample with 0.50N HCl:
[0040] The pH of the diluted supernatant was adjusted to pH=12 with 0.5N KOH, and was titrated using a RadiometerTTT 80 titrator (available from Radiometer America), a RHM 84 Research pH meter (available from Radiometer America), and an autoburette ABU80 titration system (available from Radiometer America), the supernatant was titrated with 0.50N HCl. Acid titer=volume (the number of milliliters between the two peaks of the first derivative of the titration curve)×(0.5N)×((35-(17.5×solid c...
Embodiment 1
[0046] Example 1: Preparation of Dialyzed Latex
[0047] 28 grams of the emulsion described in Emulsion 1 were processed in two separate dialysis tubing in one gallon reservoir according to the dialysis procedure described below.
Embodiment 2
[0048] Example 2: Preparation of ultrafiltered latex
[0049] Two liters of the emulsion described in Emulsion 1 were processed according to the ultrafiltration method described below.
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