Technological method for extracting lycorine from lycoris plants
A technology of lycoris and lycorine, which is applied in directions such as fermentation, and can solve problems such as unseen records and the like
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[0037] Take 150Kg of washed fresh lycoris bulbs and slice them, soak them in a functional extraction tank, add 2.1L of liquid cellulase (enzyme activity is not less than 2000u / ml), then add 600Kg of water, at a temperature of 55 ° C, pH =5, enzymolysis for 6 hours, filter after enzymolysis is completed, discard filter residue (filter residue can be used as fertilizer), get filtrate 700Kg, adjust enzymolysis solution pH9~10 with 40% sodium hydroxide aqueous solution by filtrate, make enzymolysis solution turbid , use GQ75 high-speed tubular separator to centrifugally separate and remove slag (used as fertilizer) to obtain 740Kg of centrifugate, take the centrifugate, and extract on average 6 times with 2960L ethyl acetate. , Discard the water phase, and the discarded water phase can be discharged to the sedimentation tank, adjusted to PH=7 and left for 24 hours before discharge. Concentrate the organic phase to about 15Kg with a scraper thin film concentrator, recover ethyl ace...
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