Crystallization method of abamectin Bla
A technology for crystallization of abamectin, applied in the field of crystallization of abamectin B1a, can solve problems such as inability to separate B1a and B1b, inability to take into account crystallization purity and yield, long duration, etc. Effects of caking and yield improvement
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Embodiment 1
[0022] In the spherical crystallization tank of 500ml, drop into about 40g industrial primary coarse powder (obtain by concentrating and crystallizing the leach solution that utilizes the organic solvent leaching gained to mycelia, the Abamectin B1a purity wherein is 78.21%), add 265ml normal For butanol, heat up to 80°C with stirring in a water bath, and keep the temperature constant for about 25 minutes. After it is fully dissolved, filter out the insoluble impurities while it is hot. When the clarified hot saturated solution of gained is naturally cooled to 68 ℃ in water bath, its degree of supersaturation is 1.1, adds 0.5g by the crystal seed (this crystal seed is the supersaturated solution of avermectin) by ultrasonic auxiliary preparation (prepared by applying ultrasonic waves for 20 min) stirred the solution at a speed of 100 r / min, and kept at this temperature for 20 min.
[0023] Then adjust the stirring speed to 150r / min, and lower the temperature according to the f...
Embodiment 2
[0025] In the spherical crystallization tank of 1000ml, drop into about 80g industrial primary coarse powder (obtain by concentrating and crystallizing the leach solution that utilizes the organic solvent leaching gained to mycelium, the Abamectin B1a purity wherein is 80.05%), add 600ml normal For butanol, stir in a water bath and raise the temperature to 75°C, keep the temperature for about 30 minutes, and after it is fully dissolved, filter out the insoluble impurities while it is hot. When the clear hot saturated solution of gained is naturally cooled to 65 ℃ in water bath, its degree of supersaturation is 1.3, adds 1g by the crystal seed crystal (this crystal seed is applied to the supersaturated solution of avermectin) by ultrasonic auxiliary preparation. Ultrasonic 15min), the solution was stirred at a speed of 120r / min, and kept at this temperature for 20min.
[0026] Then adjust the stirring speed to 180r / min, and lower the temperature according to the following cooli...
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