Method for preparing ferrum series non-crystalline state nanometer simple substance
A nano-element, amorphous technology, applied in the field of inorganic nano-materials, can solve the problems of poor powder particle size distribution uniformity, low efficiency, harsh reaction conditions, etc., and achieve the effects of small product particle size, simple process and equipment, and simple equipment.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0023] Prepare FeCl with a molar concentration of 0.1mol / L respectively 2 ethanol solution and KBH 4 Aqueous solution, accurately measure 0.1ml of KBH with a concentration of 0.1mol / L 4 Place the aqueous solution solution in a 1.5ml plastic centrifuge tube, add deionized water dropwise to 1ml, fasten the cap of the centrifuge tube and place it in an ultrasonic wave until a large number of bubbles appear in the solution, stop the ultrasound, take out the test tube, and open the top cover, and then quickly add 0.4ml, 0.1mol / L FeCl 2 Ethanol solution, buckle the test tube lid, quickly place the centrifuge test tube in a high-speed centrifuge, turn on the power, and adjust the acceleration of the centrifuge to 11G.
[0024] After reacting for 2-5 minutes, turn off the power, wait for the high-speed centrifuge to stop completely, take out the centrifuge test tube, a black precipitate will form at the bottom of the test tube, wash the precipitate with deionized water and alcohol f...
Embodiment 2
[0027] Prepare FeCl with a molar concentration of 0.2mol / L respectively 2 ethanol solution and KBH 4 Aqueous solution, wherein deionized water was added dropwise to 0.8ml, the acceleration of the centrifuge was adjusted to 12G, and other conditions and steps were exactly the same as in Example 1. The obtained product Fe powder is stored in absolute ethanol, and the structure and morphology of the product are characterized by XRD and TEM respectively. The obtained product has a diameter of about 12 nanometers, high product purity, and the crystal system of the product is the same as in Example 1.
Embodiment 3
[0029] Prepare NiCl with a molar concentration of 0.1mol / L respectively 2 ethanol solution and KBH 4 of aqueous solution. Other conditions and steps are exactly the same as in Example 1. Gained product Ni powder is preserved in absolute ethanol, and the structure and appearance of product are characterized by XRD and TEM respectively, as can be seen from Fig. 2, the product diameter that obtains is about 6 nanometers, and product purity is high, and product's The crystal system is the same as in Example 1.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com