Cytochrome P450 enzyme and NADPH-cytochrome P450 oxidation-reduction enzyme of crab-eating macaque
A cytochrome and cynomolgus monkey technology, applied in the field of genetic engineering, can solve problems such as no reports of cynomolgus monkey clones
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[0033]Microsomes of cynomolgus monkey P450 3A5 recombinantly expressed in sf-9 insect cells were prepared as in Example 1;
[0034] Put 0.36 mL of the mixture of microsomes, testosterone at a fixed concentration and serially diluted ketoconazole into a reaction tube, and place in a water bath at 37° C. for 5 minutes to incubate. Add 40 μL of 10 mM NADPH solution to start the reaction. After 10 minutes of reaction, add 0.8mL reaction termination solution containing internal standard to terminate the reaction, mix well and place in ice water;
[0035] The above-mentioned reaction tubes were centrifuged at 2500g for 30 minutes, and 100 μL of the supernatant was taken and added to a 96-well plate for sample injection. LC / MS / MS quantitative analysis and data processing were performed, and the activity of ketoconazole to inhibit the metabolism of testosterone by cynomolgus monkey P450 3A5 was calculated.
[0036] Cytochrome P450 enzymes and NADPH-cytochrome P450 oxidoreductase in c...
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