A pharmaceutical delivery system for deliverying active component dispersed in dispersion medium
A technology of active substance and dispersion medium, applied in the field of oral drug delivery system, which can solve the problem of narrow absorption window of active substance
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Embodiment 1
[0133] Composition according to the invention containing 50000 units of calcitonin oil dosage units
[0134] A three-layer coating composition having the shape shown in Figure 1 and containing calcitonin as active substance was prepared as follows:
[0135]
[0136] The outer plug was prepared as described in EP 0493 513 B1 with the following components:
[0137] %(w / w)
[0138] PEO 200000 60
[0139] Citric acid 5
[0140] PEG 2000ms 5
[0141] cornstarch 30
[0142] The inner plug containing calcitonin has the following composition:
[0143] %(w / w)mg
[0144] Mixed fatty acid glycerides 63 630
[0145] Corn oil 27 270
[0146] Calcitonin 10 100
[0147] While keeping the temperature below 40°C, heat the oily ingredients in a water bath until melted, then pour the melt into a mortar and cool to about 27°C with constant stirring. Add calcitonin to the melt and stir until homogeneous to obtain the inner matrix composition.
[0148] F...
Embodiment 2
[0166] Composition according to the invention containing 15,000 units of calcitonin
[0167] This composition was prepared as described above in Example 1, but with a different composition for the inner plug:
[0168] Material % (w / w) mg
[0169] Mixed fatty acid glycerides 66.8 2004
[0170] Coconut oil 28.8 864
[0171] Calcitonin 4.4 132
[0172] The composition was subjected to a dissolution test using a dissolution apparatus 2.
[0173] After about 5 hours in the artificial intestinal fluid, calcitonin began to be released (at the end of the release, the solution changed from a clear colorless solution to a cloudy solution) and ended within 1 / 2 hour.
[0174] The dosage unit has a burst release.
[0175] The composition is also tested by DSC under the following conditions:
[0176] 1) Keep at 10.00°C for 2.0min
[0177] Data Points: 120
[0178] 2) Heating from 10.00°C to 50.00°C at a rate of 15.00°C / min
[0179] Data Points: 266
[0180] Figure 7 shows the DSC ...
Embodiment 3
[0182] Composition according to the invention containing 20 mg hydrocortisone as active substance
[0183] This composition was prepared as described above in Example 1, but with a different composition for the inner plug:
[0184] Material % (w / w) mg
[0185] Mixed fatty acid glycerides 44.8 672
[0186] Corn oil 19.2 288
[0187] Hydrocortisone succinate 36 540
[0188] While keeping the temperature below 40°C, heat the oily ingredients in a water bath until melted, then pour the melt into a mortar and cool to about 27°C with constant stirring. Add hydrocortisone succinate to the melt and stir until homogeneous.
[0189] The composition was subjected to a dissolution test for 15 hours using a dissolution apparatus 1, and a dissolution curve was obtained at 273 nm with a UV detector under the conditions of 37° C. and 50 rpm.
[0190] The results are shown in Figure 8. Release of hydrocortisone succinate started after 5.5 h and ended after 1 / 2 h. The dosage unit has a b...
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Abstract
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