Process for producing bisphenol a and vertical fixed-bed reactor
A fixed-bed reactor, bisphenol technology, applied in the direction of organic chemical methods, chemical instruments and methods, preparation of organic compounds, etc., can solve the problems of acetone conversion rate decline, unavoidable degradation of sulfonic acid cation exchange resin catalyst, etc. To achieve the effect of preventing deterioration and long-term stable preparation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0036] used figure 1 The vertical fixed bed reactor shown. The bottom surface radius of reactor 1 is 2.8m, and 15% of filling sulfonic acid group is modified by 2-(4-pyridyl) ethanethiol sulfonic acid type cation exchange resin catalyst, makes catalyst layer height be 3.25m (catalyst amount : 80m 3 ). Two thermocouple thermometers 5 are arranged in the catalyst layer. Set location such as figure 1 Shown, in the horizontal direction of the catalyst layer, the distance r from the reactor periphery is the same position of 250cm, and the bottom surface of the catalyst layer in the height direction is 15cm (the distance from the bottom surface of the catalyst layer is 5%: measuring point 1= Symbol 52 in the figure) and 47 cm (14% from the bottom of the catalyst layer: measurement point 2 = symbol 53 in the figure). Furthermore, a thermocouple thermometer 6 (measuring point 0 = symbol 51 in the figure) was installed near the outlet of the reactor. Such as figure 1 As shown, i...
Embodiment 2
[0044] Use the basic structure with figure 1 The vertical fixed bed reactor shown is the same reactor. The bottom surface radius of reactor 1 is 3.3m, and 15% of filling sulfonic acid group is modified by 2-(4-pyridyl) ethanethiol sulfonic acid type cation exchange resin catalyst, makes catalyst layer height become 3.2m (catalyst amount : 110m 3 ). Two thermocouple thermometers 5 are arranged in the catalyst layer. The installation location is as follows, at the same position where the distance r from the outer circumference of the reactor is 300 cm in the horizontal direction of the catalyst layer, and 15 cm from the bottom surface of the catalyst layer in the height direction (5% from the bottom surface of the catalyst layer: measuring point 1 = symbol 52 in the figure) and 47 cm (14% from the bottom of the catalyst layer: measurement point 2 = symbol 53 in the figure). In the vertical fixed-bed reactor 1, valves 81-84 can be used to reverse the flow direction of the rea...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More