11results about How to "Stable manufacturing" patented technology

The method for preparing an amorphous silicon thin film according to the present invention includes: placing a substrate in a vacuum chamber; controlling the pressure in the vacuum chamber at a predetermined value and performing surface treatment on the substrate; and introducing silane gas and a rarefied gas into the vacuum chamber, heating the substrate, and depositing an amorphous silicon thin film on the substrate using silane gas ions. This method is characterized by low manufacturing difficulty, simple process, and low cost, while improving the growth rate and uniformity of the thin film, making the manufacturing process more stable and controllable, and resulting in a more uniform, dense, and stable amorphous silicon thin film.

The application provides a resolution method of clemastine fumarate intermediate, comprising the following steps: 1) reacting racemic N-methyl-2-(2-chloroethyl)pyrrolidine with a chiral resolving agent in a first organic solvent to obtain a diastereomeric salt solution; 2) purifying the material after the reaction in step 1) by cooling and crystallization, and filtering to obtain R-N-methyl-2-(2-chloroethyl)pyrrolidine resolving agent salt; 3) dissolving the R-N-methyl-2-(2-chloroethyl)pyrrolidine resolving agent salt obtained in step 2) in a second organic solvent-water two-phase system, adjusting the pH value to 9-13, then separating the organic phase, and concentrating to obtain R-N-methyl-2-(2-chloroethyl)pyrrolidine; wherein the chiral resolving agent is at least one selected from L-di(3,5-dinitrobenzoyl) tartaric acid and L-di-p-chlorobenzoyl tartaric acid. By using a specific chiral resolving agent, the resolution efficiency of racemic N-methyl-2-(2-chloroethyl)pyrrolidine is significantly improved, and combined with cooling and crystallization and two-phase acid adjustment replacement, the operation is simple, and the cost is controllable.

This application provides a glycourea polythiol curing agent composition, relating to the field of polymer materials technology. The composition comprises a mixture of a glycourea trithiol compound and a glycourea dithiol compound consisting of positional isomers. This composition, used as a curing agent for epoxy resin compositions, can form a highly uniform cross-linked network structure, enabling the cured epoxy resin composition to simultaneously possess a high glass transition temperature, high flexural modulus, and ultra-high fracture toughness, achieving an excellent balance between rigidity and toughness.

This invention relates to the field of welding materials technology, and particularly to a high-performance aluminum-lithium alloy flux-cored welding wire and its preparation method. The high-performance aluminum-lithium alloy flux-cored welding wire comprises: an aluminum-based metal strip outer sheath; and flux powder filled within the outer sheath. The flux powder includes deoxidizing components, alloy components, arc-stabilizing components, slag-forming components, and binding components. The alloy components of the aluminum-lithium alloy flux-cored welding wire, by mass percentage, include: Cu: 3.7%-4.3%, Li: 0.8%-1.5%, Mg: 0.25%-1%, Zr: 0.1%-0.16%, with the balance being Al and unavoidable impurities. The burn-off rate of active elements is significantly reduced, and the composition control accuracy reaches ±0.05%. The flux structure encapsulates highly active elements such as Li, Mg, and Zr in powder form within the aluminum-based outer sheath, avoiding high-temperature volatilization and oxidation in traditional smelting processes. These elements are released only during welding, achieving precise composition control and enabling the stable preparation of aluminum-lithium alloy welding wires with high Li content (2%-3%).

This invention discloses a high-performance spinning method for hollow fiber membranes and its preparation method, relating to the field of polymer membrane material preparation. The invention employs a reactive precursor system constructed from side-chain silanized polyarylether sulfone, a surface-silanized metal-organic framework, and a latent hydrophilic agent. Through a gradient reactive wet spinning process, after segmented air-gap initiation and pH-buffered solidification, an inorganic-organic interpenetrating network is constructed in situ using low-temperature solvothermal chemical crosslinking technology. The hydrophilic components are fixed through a dual mechanism of discrete ion anchoring and physical embedding. Combined with gradient solvent displacement and explosion-proof vacuum drying, this invention effectively solves the problems of pore collapse caused by high-temperature annealing, loss of physically blended fillers, and hydrophilicity degradation in traditional technologies, significantly improving the membrane's structural stability, mechanical strength, and long-term antifouling performance.

The application discloses a kind of dialkyl hypophosphite-alkyl phosphinic acid composite salt flame retardant and synthesis method thereof, it is related to organic phosphorus compound technical field, scheme is: the composite salt flame retardant is composed of dialkyl hypophosphite, alkyl phosphinic acid root and 2-4 valence metal ions;Its synthesis method includes that phosphine is added with gaseous or liquid olefin to occur radical addition, and the obtained addition product is oxidized, pH is adjusted and is salted with 2-4 valence metal salt, obtains target composite salt flame retardant.The beneficial effect of the application is: by controlling reaction ratio and subsequent conversion process, realizes the structure directional control from single salt to composite salt, so that the obtained product simultaneously has dialkyl hypophosphite and alkyl phosphinic acid root coexistence characteristics, while maintaining high conversion level, has stable preparation and good flame retardant application value.

The application provides a solute cluster reinforced aluminum alloy material and a preparation method and application thereof, and belongs to the technical field of aluminum alloy materials. The solute cluster reinforced aluminum alloy material comprises an aluminum matrix and nanometer clusters uniformly and dispersedly distributed in the aluminum matrix. The average size of the nanometer clusters is less than or equal to 5nm, the number density of the nanometer clusters is greater than or equal to 3.27*10 25 m ‑3 ; and the solute cluster reinforced aluminum alloy material is an Al-Zn-Mg-Cu alloy.

The application belongs to the technical field of silicon carbide ceramic preparation, and particularly relates to a silicon carbide ceramic slurry based on DIW-3D printing, a silicon carbide ceramic product and a preparation method. The silicon carbide ceramic slurry is prepared from raw materials including the following components and weight contents: silicon carbide mixed powder 60-100 parts, thermosetting resin 10-40 parts, dispersing agent 5-15 parts and thermal initiator 0.01-1 part. The application realizes the application of DIW-3D printing in the preparation of silicon carbide ceramic through the synergistic effect of double-particle-size SiC grading, introduction of B4C sintering aid, special resin and dispersant system, thermal initiation and solidification, DIW rheological design and gas pressure sintering, saves the material cost in the manufacturing process, prepares a silicon carbide sample with excellent mechanical properties, and further widens the development of silicon carbide ceramic.

The application discloses a kind of polybenzodifuranone and its constant potential polymerization preparation method, belong to organic conductive polymer material preparation technical field, benzodifuranone (BFDO) and supporting electrolyte are dissolved in polar aprotic solvent, and electrolyte is obtained by mixing uniformly;With platinum metal electrode as working electrode and counter electrode, with saturated calomel electrode as reference electrode, three electrodes are connected with direct current power supply and are placed in the electrolyte, in air atmosphere, electrochemical polymerization reaction is carried out using constant potential method;After reaction, the reaction liquid is extracted and filtered, dried, to obtain polybenzodifuranone (PBFDO).The application uses constant potential electrochemical polymerization method, n-type conductive polymer polybenzodifuranone can be synthesized in air atmosphere in one step, without catalyst, high-temperature anaerobic environment and complex post-processing, the product conductivity is 1.157-18.28 S / cm.Process simplification, low cost, process controllable, can realize green scale preparation and industrialization application.

This invention belongs to the field of piezoelectric materials and discloses a lead nickel tungstate-lead zirconate titanate piezoelectric ceramic and its preparation method. The general chemical formula of the lead nickel tungstate-lead zirconate titanate piezoelectric ceramic of this invention is: xPb(Ni 1 / 2 W 1 / 2 )O3-yPbZrO3-(1-x-y)PbTiO3+zwt%MnO2; where, 0.05

This invention discloses a device for fixing and trimming autologous bone grafts for dental implants, belonging to the field of dental medical device technology. The device includes a first clamping arm and a second clamping arm; the first and second clamping arms are hinged together by fasteners to form a scissor-like lever structure; the first clamping arm includes a first gripping part and a first clamping section, the first clamping section being connected to a positioning frame; the second clamping arm includes a second gripping part and a second clamping section; the second clamping section is connected to a movable pressure plate; the positioning frame and the movable pressure plate are arranged opposite to each other and together enclose a bone placement cavity for accommodating and fixing the autologous bone graft. This invention adopts an integrated design, integrating four core functions—stable clamping, anti-slip fixation, precise cutting guidance, and pre-positioning of bone screw holes—into a single handheld instrument, achieving a "one-stop" precise, efficient, and stable preparation from bone graft to ready-to-use bone graft.