Agglutinate neodymium-iron-boron magnet and preparation method thereof
A neodymium iron boron and magnet technology, used in magnetic objects, inductance/transformer/magnet manufacturing, magnetic materials, etc., can solve problems such as process and product performance defects, mechanical performance deterioration, etc., to achieve favorable mechanical strength, mold release and The effect of good dimensional precision
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Embodiment 1
[0012] Weigh MQP-B 80mesh magnetic powder 10,000g, EPON 840 bisphenol A epoxy resin (epoxy equivalent EEW=330-380) 100g, dicyandiamide 3.662g, 3-(3,3-dichlorophenyl)-1 , 1-dimethylurea 1.831g, Wacker H 20 Silica 20g, acetone 1000g, the above-mentioned components are prepared into resin solution, mixed with planetary mixer for 15 minutes under nitrogen environment, dried under 55 degrees Celsius for 120 minutes with blast oven, removed acetone, and obtained containing nano-silica magnetic powder - Resin mix. Use Lakeshore 7312 VSM (Vibrating Sample Magnetometer) tester to test the magnetic properties of the obtained magnetic powder-resin mixture; use YA-20 electro-hydraulic pressure testing machine to examine the demoulding force of the obtained magnetic powder-resin mixture; use Gasbarre 15T press at 14ton / cm 2 Pressed under pressure into a ring magnet green body with an outer diameter of 20.80mm and an inner diameter of 18.60mm; cured at a constant temperature of 170 degre...
Embodiment 2
[0014] Weigh MQP-B 80mesh magnetic powder 10,000g, EPON 840 bisphenol A epoxy resin (EEW=330-380) 100g, dicyandiamide 3.662g, 3-(3,3-dichlorophenyl)-1,1- Dimethylurea 1.831g, Wacker H 20 10 g of silicon dioxide, 1000 g of tetrahydrofuran, the above-mentioned components are prepared into a resin solution, mixed with a planetary mixer for 15 minutes in a nitrogen environment, and dried for 120 minutes under a condition of 65 degrees Celsius in a blast oven to remove the tetrahydrofuran to obtain nano-silica reinforced. Magnetic powder-resin mixture. The magnetic properties of the obtained magnetic powder-resin mixture were tested by a Lakeshore7312 VSM (Vibrating Sample Magnetometer) tester; the demolding force of the obtained magnetic powder-resin mixture was investigated by a YA-20 electro-hydraulic pressure testing machine; a Gasbarre 15T press was used at 14ton / cm 2 Pressed under pressure into a ring magnet green body with an outer diameter of 20.80mm and an inner diamete...
Embodiment 3
[0016] Weigh MQP-B 80mesh magnetic powder 10,000g, EPON 840 bisphenol A epoxy resin (EEW=330-380) 100g, dicyandiamide 3.662g, 3-(3,3-dichlorophenyl)-1,1- Dimethylurea 1.831g, Wacker H 20 Silica 3g, acetone: tetrahydrofuran=1:1 wt% mixed solution 1000g, the above components were prepared into resin solution, mixed for 15 minutes with a planetary mixer under a nitrogen environment, and dried under a blast oven at 60 degrees Celsius for 120 minutes to remove solvent to obtain a nano-silica reinforced magnetic powder-resin mixture. Use Lakeshore 7312 VSM (Vibrating Sample Magnetometer) tester to test the magnetic properties of the obtained magnetic powder-resin mixture; use YA-20 electro-hydraulic pressure testing machine to examine the demoulding force of the obtained magnetic powder-resin mixture; use Gasbarre 15T press at 14ton / cm 2 Pressed under pressure into a ring magnet green body with an outer diameter of 20.80mm and an inner diameter of 18.60mm; cured at a constant tem...
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