Ink for inkjet recording, ink set for inkjet recording, ink media set for inkjet recording, ink cartridge, inkjet recording method, and inkjet recording apparatus
A technology for inkjet recording, recording medium, applied in the direction of copying/marking method, ink, application, etc.
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preparation Embodiment 1
[0285] -Preparation of surface-treated carbon black pigment dispersion-
[0286] In 3000mL 2.5N sodium sulfate solution, add 90g CTAB with a surface area of 150m 2 / g, and the DBP oil absorption is 100ml / 100g of carbon black, and the mixture was stirred at 300rpm at 60°C for 10 hours, whereby the mixture was reacted and oxidized. The obtained reaction liquid was filtered, and carbon black obtained from the filtrate was neutralized by using sodium hydroxide, followed by ultrafiltration. The carbon black thus obtained was washed with water, then dried, and then dispersed in pure water so that the dispersion contained 20% by mass of carbon black.
preparation Embodiment 2
[0288] -Preparation of Surface-Treated Yellow Pigment Dispersion-
[0289] C.I. Pigment Yellow 128 was subjected to low-temperature plasma treatment to produce a pigment into which a carboxylic acid group was introduced as a yellow pigment. The pigment thus obtained was dispersed in ion-exchanged water, and the dispersion was subjected to desalination concentration by using an ultrafiltration membrane, whereby a yellow pigment dispersion having a pigment concentration of 15% was prepared.
preparation Embodiment 3
[0291] -Preparation of surface-treated magenta pigment dispersion-
[0292] A surface-treated magenta pigment was prepared in the same manner as in Preparation Example 2, provided that C.I. Pigment Red 122 was used instead of C.I. Pigment Yellow 128. Similar to the case of Preparation Example 2, the surface-treated pigment was easily dispersed in an aqueous medium when stirred, and the dispersion was desalted and concentrated by using an ultrafiltration membrane, thereby obtaining a magenta color with a pigment concentration of 15%. Pigment dispersions.
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