Apple juice
An apple juice and beverage technology, applied in the field of beverages, can solve the problems of drinking within an hour, waste, easy deterioration of apple juice, etc., and achieve the effect of improving the shelf life and improving the shelf life.
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Embodiment 1
[0017] 1. The preparation of the preservative includes the following steps:
[0018] a) pulverization process: the orange peel is washed, and pulverized into particle size of 20 meshes;
[0019] b) alcohol extraction process: adding 5 times of the total weight of orange peel is 60% ethanol, soaking for 20 hours, and filtering;
[0020] c) Concentration process: the extract prepared in the alcohol extraction process is concentrated to a density of 1.05 g / cm 3 the extract;
[0021] d) purification process: the extract prepared in the concentration process is subjected to column chromatography with silica gel, and eluted with an eluent. The weight ratio of the extract to the silica gel is 1:2, and the eluent is ether, ethyl acetate, and ammonia. The volume ratio of the mixture is 1:0.5:0.01.
[0022] e) Collection process: the components of the second color band are collected, and the collected material is subjected to vacuum distillation under the condition of a water bath te...
Embodiment 2
[0025] 1. The preparation of the preservative includes the following steps:
[0026] a) pulverization process: the orange peel is washed, and pulverized into particle size of 60 meshes;
[0027] b) alcohol extraction process: adding 70% ethanol with a volume concentration of 8 times the total weight of orange peel, soaking for 15 hours, and filtering;
[0028] c) Concentration process: the extract prepared in the alcohol extraction process is concentrated to a density of 1.1 g / cm 3 the extract;
[0029] d) purification process: the extract prepared in the concentration process is subjected to column chromatography with silica gel, and eluted with an eluent. The weight ratio of the extract to the silica gel is 1:2.5, and the eluent is ether, ethyl acetate, and ammonia. The volume ratio of the mixture is 1:0.7:0.03.
[0030] e) Collection process: the components of the second color band are collected, and the collected material is subjected to vacuum distillation under the co...
Embodiment 3
[0033] 1. The preparation of the preservative includes the following steps:
[0034] a) pulverization process: the orange peel is washed, and pulverized into particles with a particle size of 100 meshes;
[0035] b) alcohol extraction process: adding 5 times of the total weight of orange peel is 95% ethanol, soaking for 10 hours, and filtering;
[0036] c) Concentration process: the extract prepared in the alcohol extraction process is concentrated to a density of 1.2 g / cm 3 the extract;
[0037] d) purification process: the extract prepared in the concentration process is subjected to column chromatography with silica gel, and eluted with an eluent. The weight ratio of the extract to the silica gel is 1:2.5, and the eluent is ether, ethyl acetate, and ammonia. The volume ratio of the mixture is 1:0.8:0.05.
[0038] e) Collection process: the components of the second color band are collected, and the collected material is subjected to vacuum distillation under the condition...
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