Flavouring essences for tobacco and preparation thereof
A technology of tobacco flavor and methylvaleric acid, which is applied in the field of tobacco flavor, can solve the problems of bad influence of cigarette smoke, unpleasant smell, uneven volatilization, etc. air quality effect
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[0016] Essence for tobacco of the present invention, take 3-methylpentanoic acid and menthol as raw material, and reaction formula is as follows:
[0017]
[0018] The substance ratio of 3-methylpentanoic acid to menthol is 1.5:1.
[0019] The preparation method of flavoring essence for tobacco of the present invention comprises the following steps: using 3-methylvaleric acid and menthol as raw materials, wherein, the ratio of substances of 3-methylvaleric acid to menthol is 1.5:1, and using benzene As a water-carrying agent, the catalyst is p-toluenesulfonic acid, the reaction heating temperature is 130°C, the reaction time is 5h, and the reaction produces menthyl 3-methylvalerate, wherein the consumption of the catalyst p-toluenesulfonic acid is The reactant 3-methylpentanoic acid and menthol substances amount and 3%.
[0020] Characterization of the prepared product
[0021] Infrared Spectroscopy (IR)
[0022] The prepared reaction product was subjected to infrared sp...
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