Treatment technology of accompanying gas in production process of trichlorosilane
An associated gas and production process technology, applied in the directions of halogenated silanes, halogenated silicon compounds, combined devices, etc., can solve the problems of polluted air and associated gas emissions, and achieve the effect of reducing pollution and production costs.
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Embodiment 1
[0008] ①Dust removal: the associated gas during the production of trichlorosilane is recovered and reused in the dust removal equipment to initially purify the associated gas;
[0009] ②Leaching: In the two-stage leaching tower, under high temperature conditions, the associated gas after preliminary purification is rinsed with silicon tetrachloride, and the silicon powder that has not been cleaned of the associated gas is absorbed into the silicon tetrachloride solution;
[0010] ③Precipitation: Precipitate the leached silicon tetrachloride solution in the precipitation tank for harmless treatment;
[0011] ④Gas separation: freezing and separating the associated gas after leaching, and then compressing and freezing the separated gas with a compressor;
[0012] ⑤ Absorption: The gas after compression and freezing separation is sent to the hydrogen chloride separation tower to absorb the hydrogen chloride contained in the gas, and then the hydrogen is adsorbed and purified;
[0013] ⑥Exha...
Embodiment 2
[0015] After the leached silicon tetrachloride solution is precipitated in the precipitation tank, the silicon tetrachloride solution is sent to the rectification tower for rectification and reuse.
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