Process for manufacturing polishing pad
一种制造方法、研磨垫的技术,应用在研磨机床、制造工具、研磨工具等方向,能够解决无法采用、浆料泄漏等问题
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preparation example Construction
[0064] An example of the production method of the cell-dispersed urethane composition will be described below. The preparation method of the bubble-dispersed urethane composition includes the following steps.
[0065] 1) Foaming process for preparing a bubble dispersion liquid of isocyanate-terminated prepolymer
[0066] A polysiloxane-based surfactant is added to the isocyanate-terminated prepolymer (first component), followed by stirring in the presence of a non-reactive gas to disperse non-reactive air cells as fine air cells to obtain an air cell dispersion. When the prepolymer is solid at normal temperature, it is used after being preheated to an appropriate temperature and melted.
[0067] 2) Curing agent (chain extender) mixing process
[0068] A chain extender (second component) was added to the above-mentioned cell dispersion liquid, followed by mixing and stirring to prepare a cell-dispersed urethane composition.
[0069] As the non-reactive gas for forming microb...
Embodiment
[0119] Hereinafter, the present invention will be described with reference to examples, but the present invention is not limited to these examples.
[0120] (Asker D hardness measurement)
[0121] Performed in accordance with JIS K6253-1997. A light transmission region cut into a size of 2 cm×2 cm (thickness: optional) was used as a sample for hardness measurement. In addition, a water-impermeable membrane was prepared from the polyurethane resin paint used in Examples 1, 2 and Comparative Example 1, and cut into a size of 2 cm x 2 cm (thickness: optional) as a sample for hardness measurement. In addition, the PET base material used in Comparative Example 2 was cut into a size of 2 cm×2 cm (thickness: optional), and used as a sample for hardness measurement. These measurement samples were left to stand in an environment with a temperature of 23°C±2°C and a humidity of 50%±5% for 16 hours. During the measurement, the samples were stacked so that the thickness was 6 mm or mor...
manufacture example
[0136] 32 parts by weight of toluene diisocyanate (2,4-form / 2,6-form=80 / 20 mixture), 8 parts by weight of 4,4'-dicyclohexylmethane diisocyanate, 54 parts by weight of polytetramethylene glycol ( Number average molecular weight: 1006) and 6 parts by weight of diethylene glycol were mixed, heated and stirred at 80° C. for 120 minutes to produce an isocyanate-terminated prepolymer (isocyanate equivalent: 2.1 meq / g). 100 parts by weight of the isocyanate-terminated prepolymer and 3 parts by weight of a polysiloxane-based surfactant (manufactured by Toray Dazu Corning Silicone Co., Ltd., SH-192) were mixed to prepare a mixture whose temperature was adjusted to 80°C. 80 parts by weight of this mixture and 20 parts by weight of 4,4'-methylene bis(o-chloroaniline) (manufactured by Ihara Chemical Co., Ltd., Ihara Kyuamin MT) melted at 120° C. were mixed in a mixing chamber while air was dispersed in the mixture by mechanical stirring. In the mixture, a cell-dispersed urethane compositi...
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