Anti-human progastrin polypeptide immune composition
An immune composition and peptide-mimicking technology, applied in hormone peptides, drug combinations, gastrin/cholecystokinin, etc., can solve the problem of not being able to capture gastrin
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Embodiment 1
[0015] Peptides were synthesized using standard solid-phase synthesis methods. The amino acid content and purity of each polypeptide were identified using methods commonly used in the art.
[0016] Synthesize a polypeptide with the following amino acid sequence:
[0017] The amino acid sequence of peptide: 1) Cys-pro-Pro-Pro-Pro-Ser-Ser-Gly-Trp-Met-Asp-Phe-Gly-Arg-Arg-Ser-Ala-Glu-Asp-Glu-Asn (SEQ ID NO.: 1) (G-21); 2) pGlu-Gly-Pro-Trp-βLeu-Glu-Glu-Glu-Glu-Glu-Ala-Ser-Ser-Pro-Pro-Pro-Pro-pro-Cys( SEQ ID NO.: 2) (G-18); 3) (hu G17 homologue) pGlu-Gly-Pro-Trp-βLeu-Glu-Glu-Glu-Glu-Glu-Ala-Ser-Ser-Pro- Pro-Pro-pro-Cys (SEQ ID NO.: 3) (G-18LV); 4) pGlu-Gly-Pro-Trp-Ile-Glu-Glu-Glu-Glu-Glu-Ala-Ser-Ser-Pro - Pro-Pro-pro-Cys (SEQ ID NO.4) (G18LI); 5) Cys-pro-Pro-Pro-Pro-Trp-Leu-Glu-Glu-Glu-Glu-Glu-Ala-Tyr-Gly -Trp-Met-Asp-Phe-Gly; (SEQ ID No.5)(G-20a); 6) Cys-pro-Pro-Pro-Pro-Trp-Leu-Glu-Glu-Glu-Glu-Glu- Ala-pNO 2 -Phe-Gly-Trp-Met-Asp-Phe-Gly; (SEQ ID No.6)(G-20b); 7) Ser-Ser-Pro-P...
Embodiment 2
[0025]The polypeptide-TT cross-linked product in Example 1 was emulsified for immunization, and the preparation method of the emulsion was as follows: the concentration of the cross-linked product and adjuvant in the aqueous phase was twice the concentration in the final emulsion. , the cross-linked product was dissolved in PBS with a pH of 6.5-8 to make a final concentration of 5-12 mg / ml. The aqueous and oily media were mixed 1:1 (v / v) to form an emulsion containing the final immunogen. Various types of oily media known to those skilled in the art can be used. One of the oil phase medium is composed of 20-60 parts of squalene, 70-30 parts of squalane, 2-12 parts of Span 80, 0.6-2 parts of lead monostearate, 0.1-1 part of Tween 80 and 0.2-1.2 parts Tween 40 mixed. The aqueous and oily phases can be mixed by any means known to those skilled in the art to form an emulsifying mixture. The emulsifier must be stable during storage (e.g. no significant separation of the oil and ...
Embodiment 3
[0028] As described in Examples 1 and 2, we used the peptides G18 and G21 in Example 1 to link with TT and DT, respectively, to construct conjugates, and then immunogen with peptide G18 ( Figure 1A , 1B) and peptide G21 immunogen ( Figure 1C , 1D) Six mice were immunized respectively.
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