Modified fatty acid ester, preparation method and application thereof

A fatty acid ester and fatty acid technology, applied in the field of drilling fluid treatment agent, can solve the problems of high lubricant cost, high freezing point, inconvenient use, etc. Lubricity effect

Inactive Publication Date: 2012-09-05
濮阳市诚信钻采助剂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Some directly use oleic acid as a drilling fluid lubricant, which has a good lubricating effect, but severe foaming during use has a great impact on other properties of the drilling fluid. After use, the drilling fluid needs to be followed up. It brings great inconvenience; some are modified with vegetable oils such as palm oil and cottonseed oil, but the freezing point is too high, so it is extremely inconvenient to use in winter
For the reduction of the extreme pressure lubrication coefficient, the currently used products generally can only reach 50% to 80%. Even if a large amount of drilling fluid lubricant is added to the drilling fluid, it still cannot meet the needs of complex wells
In addition, the cost of preparing drilling fluid lubricants from vegetable oil is relatively high, and compared with crude oil, the cost performance has no advantage

Method used

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Embodiment Construction

[0020] The modified fatty acid ester comprises the following raw materials in parts by weight: 1000-2000 parts of vegetable fatty acid, 50-250 parts of sulfuric acid, 20-150 parts of nitric acid, 100-800 parts of methanol, 10-100 parts of surfactant, 25-100 parts of quicklime share. Wherein the catalyst is sulfuric acid, and the surfactant is Span80. The molecule of the vegetable fatty acid contains an adsorption group.

[0021] The preparation method of described modified fatty acid ester comprises the following steps:

[0022] (1) select the raw material of above-mentioned weight portion for subsequent use;

[0023] (2) Add vegetable fatty acid and waste acid water produced in the follow-up process to the reaction kettle, heat up to 50-180°C, react for 2-8 hours, then let it stand for 1-5 hours, and separate the water to obtain refined fatty acid;

[0024] (3) Add nitric acid to the prepared refined fatty acid, keep the temperature in the reaction kettle at 50-120°C for 3...

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Abstract

The invention relates to a drilling fluid finishing agent applied to the petroleum and natural gas drilling engineering, as well as a preparation process and application thereof. The modified fatty acid ester comprises the following raw materials in parts by weight: 1000 to 2000 parts of vegetable fatty acid, 50 to 250 parts of catalyst, 20 to 150 parts of nitric acid, 100 to 800 parts of methanol, 10 to 100 parts of surfactant and 25 to 100 parts of calcined lime. The modified fatty acid ester is used as the anti-seize lubricant of the drilling fluid. The invention has the advantages of low cost of the raw material, no pollution to the environment in the preparation process of the product, good lubricating property and no influence to the discovery of the oil-gas reservoir.

Description

Technical field: [0001] The invention relates to a drilling fluid treatment agent used in petroleum and natural gas drilling engineering, as well as its production process and application. Background technique: [0002] In oil and gas drilling engineering, drilling fluid plays a vital role, one of which is to lubricate drill bits and drilling tools and increase drilling speed. Therefore, drilling fluid lubricants have always been a research hotspot. [0003] Drilling fluid lubricants made of artificial synthesis and oil modification have gradually become the mainstream of drilling fluid lubricants since the 1990s. Some directly use oleic acid as a drilling fluid lubricant, which has a good lubricating effect, but severe foaming during use has a great impact on other properties of the drilling fluid. After use, the drilling fluid needs to be followed up. Bring great inconvenience; Some are modified with vegetable oils such as palm oil and cottonseed oil to make, but the fre...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/035
Inventor 孙金声张兰英李旭东胡树林
Owner 濮阳市诚信钻采助剂有限公司
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