Method for preparing step standard sample of nano-scale oxide crystalloid with high precision

A nano-scale oxide, standard sample technology, applied in the preparation of test samples, measuring devices, instruments, etc., can solve the problems of poor stability of crystal plane steps, easy to be oxidized, etc., and achieve high stability, variety, and shape. rich effects

Inactive Publication Date: 2010-08-25
TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This invention describes different ways for creating high-quality small particles that can be used in electronic devices or other applications such as catalysts. These tiny objects show great promise due their unique shape, size ranges, and stable properties over time.

Problems solved by technology

This patented technical problem addressed in this patents relates to improving the precision and reproducibility of measuring small dimensions accurately at submicrons levels over large distances. Current techniques involve expensive instrumentations like X-ray fluorescence spectroscopy and electron beam probes, but they cannot achieve required specific values due to instability caused by environmental factors during manufacture. To address this issue, researchers developed new ways called Surface Scan Calibrator Standard Sets (SCFS). These tools include silane films made up mostly of hydrogen atoms bonded together through strong bonds between them, resulting in improved stability compared to previous methods involving organics. Additionally, there was an attempt to create minute terraces instead of traditional step plugs based upon oxynaphthene patterns formed inside the wafer's surface. By doing this, the size of each step becomes larger without compromising its reliability. Overall, these improvements aim to improve the performance and quality control of nanoposition measurements while maintaining cost efficiency.

Method used

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  • Method for preparing step standard sample of nano-scale oxide crystalloid with high precision
  • Method for preparing step standard sample of nano-scale oxide crystalloid with high precision
  • Method for preparing step standard sample of nano-scale oxide crystalloid with high precision

Examples

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Embodiment 1

[0023] Tungstate crystal KLu(WO 4 ) 2 It is an excellent laser crystal with stable physical and chemical properties and mature growth technology. This embodiment uses tungstate crystal KLu (WO 4 ) 2 (110) Surface natural steps make nanoscale step height standard samples, the steps are as follows:

[0024] 1) Use an X-ray orientation instrument to orient each naturally exposed surface of the tungstate crystal, determine the crystal plane Miller index of each naturally exposed surface, and select a naturally exposed surface (110) of the tungstate crystal as Naturally exposed base surface;

[0025] 2) Cut the tungstate crystal in a direction parallel to the base surface of the natural exposure surface to obtain three square oxide crystals with a thickness of 1mm and a base surface of the natural exposure surface and a cutting exposure surface; the square tungsten The crystal sizes of acid salts are 3mm×3mm, 5mm×5mm and 10mm×10mm;

[0026] 3) Grinding and polishing the cuttin...

Embodiment 2

[0029] Using tungstate crystal KLu(WO 4 ) 2 (310) surface natural steps to make standard samples of nanoscale step heights.

[0030] The oxide crystals used and the sample preparation process were the same as in Example 1, except that the selected natural exposed surface was the (310) surface, the thickness of the cut sample was 2mm, and the size was 2mm×2mm.

[0031] Fig. 2 is the straight step row on the surface of the standard sample (310), the step height is 0.2800nm.

[0032] According to this procedure and method, we can prepare standard samples with a step height of 0.2800nm ​​on a large scale.

Embodiment 3

[0034] Using borate crystal La 2 CaB 10 o 19 (001) surface natural steps to make standard samples of nanoscale step heights. La 2 CaB 10 o 19 It is an excellent nonlinear optical crystal invented by the Chinese Academy of Sciences. It has stable physical and chemical properties, no deliquescence, and easy storage.

[0035] The sample preparation process is the same as in Example 1, the difference is that the oxide crystals used are borate crystals La 2 CaB 10 o 19 , the selected natural plane is the (001) plane of the crystal, the thickness of the cut sample is 0.5mm, and the size is 5mm×5mm.

[0036] Fig. 3 is the monomolecular layer step on the surface of the standard sample (001), and the step height is 0.9126nm.

[0037] According to this procedure and method, standard samples with a step height of 0.9126nm can be prepared on a large scale.

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Abstract

The invention relates to a method for preparing a step standard sample of a nano-scale oxide crystalloid with the high precision, comprising the following steps of: (1) orienting each natural exposing surface of an oxide transistor by using an X-ray orientation device, determining Miller indices of crystal surfaces of each natural exposing surface and selecting one natural exposing surface of the oxide crystalloid as a base plane of the natural exposing surface; (2) cutting the oxide crystalloid in a direction parallel to the base plane of the natural exposing surface to obtain a square oxide crystalloid having the base plane of the natural exposing surface and a cutting exposing surface; and (3) grinding and polishing the cutting exposing surface of the square oxide crystalloid so that the cutting exposing surface is parallel to the base plane of the natural exposing surface, and then searching the step on the base plane of the natural exposing surface of the square oxide crystalloid by using an atomic force microscope to obtain the step standard sample of the nano-scale oxide crystalloid with the high precision. The step height standard sample manufactured by the method has the advantages of favorable stability, wide step height range, simple operation, low cost, high precision and the like.

Description

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Claims

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Application Information

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Owner TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI
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