Method for preparing release-type metal vapour-phase rust preventative

A gas-phase anti-rust agent, slow-release technology, applied in the field of preparation of slow-release metal gas-phase anti-rust agents, can solve the problems of loss of anti-rust function, anti-rust failure, anti-rust space cannot be completely sealed, etc., to achieve anti-rust The effect of prolonging the time and improving the heating capacity

Inactive Publication Date: 2010-09-29
XIANYANG DEBANG CHEM ENG TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in reality, the situation that the anti-rust space cannot be completely sealed exists completely, so the anti-rust failure is often caused, or new anti-rust agents need to be replenished regularly, which increases the cost of anti-rust
Especially the antirust agent used for vapor phase antirust paper must be dissolved into a solution and then dried after being coated on the paper. At this time, the usual antirust agent will be volatilized and decomposed due to high temperature, and part of the antirust function will be lost.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Example 1: Dissolve β-cyclodextrin in water at 50°C to make a saturated solution; keep the above temperature constant, add β-cyclodextrin to the saturated solution under stirring: metal vapor phase rust inhibitor = 1.5 : Add metal vapor phase rust inhibitor at a mass ratio of 1, and perform clathrate reaction for 80 minutes; after the reaction is stopped, the solution is freeze-dried to obtain a powder that is the required slow-release metal vapor phase rust inhibitor, and finally the slow-release metal vapor phase rust inhibitor The rust agent is processed into tablets.

Embodiment 2

[0017] Example 2: Dissolve carboxymethyl β-cyclodextrin in water at 55°C to make a saturated solution; maintain the above temperature, add carboxymethyl β-cyclodextrin to the saturated solution under stirring: metal Vapor-phase antirust agent=2:1 mass ratio, add metal vapor-phase antirust agent, clathrate reaction for 85 minutes; after stopping the reaction, freeze-dry the solution to obtain powder which is the required slow-release metal vapor-phase antirust agent, and finally put this The slow-release metal vapor phase rust inhibitor is processed into powder.

Embodiment 3

[0018] Example 3: Dissolve hydroxypropyl β-cyclodextrin in water at 60°C to make a saturated solution; maintain the above temperature, add hydroxypropyl β-cyclodextrin to the saturated solution under stirring: metal Vapor-phase antirust agent=1:1 mass ratio, add metal vapor-phase antirust agent, clathrate reaction for 90 minutes; after stopping the reaction, freeze-dry the solution to obtain powder, which is the required slow-release metal vapor-phase antirust agent, and finally put this The slow-release metal vapor phase rust inhibitor is processed into a liquid.

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PUM

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Abstract

The invention relates to a method for preparing environment-friendly release-type metal vapour-phase rust preventative. By means of the effect that cyclodextrin can well include and slowly release the medicament, the medicament includes the active ingredients in vapour-phase rust preventative in cavity of beta-cyclodextrin or a derivative of the beta-cyclodextrin. The mass ratio of the used beta-cyclodextrin or the derivative of the beta-cyclodextrin to the metal vapour-phase rust preventative is 1-2:1. The product can be made into powder, liquid or tablets, directly used for metal rust prevention and particularly used for manufacturing of anti-rust papers and plastic anti-rust films. The product has the following advantages that: 1, the product is safe, environment-friendly and convenient; 2, the product has long-acting and slow-release effect and the rust protection time can be greatly prolonged; and 3, the product can improve the stability and the heat-bearing capacity for the rust preventative and is particularly suitable for the process for manufacturing the anti-rust papers and the plastic anti-rust films.

Description

technical field [0001] The invention relates to a preparation method of an antirust agent, in particular to a preparation method of a slow-release metal vapor phase antirust agent. Background technique [0002] Metal is the most important structural material in modern machinery industry, national defense industry and other departments. It is easily corroded by the chemical and electrochemical effects of the external environment. Atmospheric corrosion is the most widespread kind of corrosion, and the loss caused by it accounts for more than half of the total corrosion loss. According to reports, China's annual economic loss due to metal corrosion is about 280 billion yuan. For this reason, people adopt various methods to protect metal products, such as coating protective sealing method, desiccant method, vacuum antirust sealing method, inert gas protection method and gas phase antirust method, etc. [0003] A lot of practice has proved that vapor phase antirust packaging is...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23F11/02
Inventor 陈均志付雨生邵超群张桂香付喜军
Owner XIANYANG DEBANG CHEM ENG TECH
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