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Reactor for producing biodiesel in presence of solid catalyst

A solid catalyst, biodiesel technology, applied in chemical/physical processes, chemical instruments and methods, etc., can solve problems such as reducing equipment utilization, affecting conversion rate, insufficient contact between reaction substrate and catalyst, and extending service life. , the effect of convenient reuse

Inactive Publication Date: 2010-12-29
上海绿铭环保科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when using solid catalysts (including solid catalysts such as immobilized biological enzymes, acids, alkalis, and salts) as catalysts, there are some shortcomings in simply using traditional reactors, which are mainly manifested in the following two points: 1. Catalyst reuse is extremely low convenient
After the catalytic reaction is over, the reaction solution needs to be pumped out of the reactor to filter out the catalyst. When it is used next time, the filtered catalyst is put back into the reactor for catalytic reaction, which not only increases the production operation time, but also reduces the cost of equipment. Utilization rate, wasted human resources again; Two, solid catalyst density is greater than water, easily deposits on the bottom of the reactor, although the reactor can be provided with baffles, the longitudinal mass transfer of the reaction solution is still not ideal, so that the reaction substrate and Insufficient catalyst contact affects conversion rate

Method used

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  • Reactor for producing biodiesel in presence of solid catalyst
  • Reactor for producing biodiesel in presence of solid catalyst
  • Reactor for producing biodiesel in presence of solid catalyst

Examples

Experimental program
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Embodiment 1

[0019] Such as figure 1 As shown, it is a reactor for the production of biodiesel catalyzed by a solid catalyst. The reactor is a stirred tank reactor 10. In the stirred tank reactor 10, there are two built-in filters that open downward and extend out of the tank. Devices 13 and 14, each built-in filter is provided with a layer of filter screen, and the mesh of the filter screen is smaller than the particle size of the solid catalyst particle for reaction, which can stop the catalyst from leaking from the built-in filter 13 and the filter 14. The circulation pump in this embodiment is a centrifugal mixing pump 50 which has an inlet 501 , an inlet 502 and a total outlet 503 . The built-in filter 13 communicates with the pipeline 2 and the recoil pipeline 1; the built-in filter 14 communicates with the pipeline 3 and the recoil pipeline 4; And recoil pipeline 4 is communicated with the total outlet 503 of centrifugal mixing pump 50; Feed port 11 is communicated with the total o...

Embodiment 2

[0023] Another embodiment of the present invention is formed after the above-mentioned equipment is changed, such as figure 2 As mentioned above, the methanol storage tank 40 can be directly communicated with another feed port 11 of the stirred tank reactor 10 through the pipeline 41. At this time, the circulation pump is a common pump 70, and the inlet 701 of the pump 70 is connected to the pipeline 2 of the outlet of the filter. The pipeline 3 is connected; the outlet 702 of the pump 70 is connected with the recoil pipeline 1 of the filter, the backflush pipeline 4, and the pipeline 5, and the pipeline 5 is connected with the feed port of the stirred tank.

[0024] Similarly, use figure 2 The equipment shown produces biodiesel that differs from figure 1 The first step is to directly add the methanol in the methanol storage tank 40 to the stirred tank reactor 10 without transporting it through an external circulation pump. the rest with figure 1 The steps for using the e...

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PUM

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Abstract

The invention relates to a reactor for producing biodiesel in the presence of a solid catalyst. The reactor comprises a stirring tank, a filter, a circulating pump, a methanol storage tank and a discharging pump, wherein the filter is internally arranged at the bottom of the stirring tank; the outlet of the filter is connected with the inlet of the circulating pump; the outlet of the circulating pump is connected with the feed inlet of the stirring tank; the stirring tank is connected with the outlet of the circulating pump through a pipeline with a control valve; and the methanol storage tank is directly connected with the feed inlet of the stirring tank or the inlet of the circulating pump. Compared with the prior art, the reactor has the advantages of conveniently recovering the solid catalyst, prolonging the service life of the catalyst, reducing the cost, and the like.

Description

technical field [0001] The invention relates to a reactor for producing biodiesel, in particular to a reactor for catalyzing the production of biodiesel by a solid catalyst (including solid catalysts such as immobilized biological enzymes, acids, alkalis, salts, etc.). Background technique [0002] Currently, conventional stirred tank reactors, packed column reactors, or airlift reactors are commonly used in biodiesel production using solid catalysts. Among the three reactors, the stirred tank reactor has the best mass transfer effect and is currently the most widely used. However, when using solid catalysts (including solid catalysts such as immobilized biological enzymes, acids, alkalis, and salts) as catalysts, there are some shortcomings in simply using traditional reactors, which are mainly manifested in the following two points: 1. Catalyst reuse is extremely low Convenience. After the catalytic reaction is over, the reaction solution needs to be pumped out of the re...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/10
Inventor 端木勉聂开立周位邓利谭天伟叶正尧
Owner 上海绿铭环保科技股份有限公司
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