Polymerizable composition
A polymer composition, polymer technology, applied in the direction of graft polymer adhesives, adhesive types, coatings, etc.
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[0208] 1. Fabrication of Core-Shell Particles
[0209] 1.1 Manufacturing of nuclei
[0210] Reagents used:
[0211] Butyl Acrylate Acros 99%, CAS 141-32-2
[0212] Ammonium Lauryl Sulfate Disponil ALS 33, 33% in water, Cognis
[0213] Tripropylene glycol diacrylate Laromer TPGDA, BASF SE
[0214] Potassium peroxodisulfate Merck
[0215] A mixture of 0.92 g Disponil ALS 33 in 241 g water was homogenized with vigorous stirring in a beaker. To this mixture was added a mixture of 60.20 g of butyl acrylate and 0.061 g of tripropylene glycol diacrylate in 4.02 g of water, and the resulting mixture was homogenized with vigorous stirring. The homogeneous mixture was treated 4 times with a Microfluidizer (Microfluidics Co.) at 8000 psi to make a microemulsion.
[0216] A stream of nitrogen was injected into the resulting mixture at room temperature for 25 minutes. After heating to 75°C, 0.063 g of potassium peroxodisulfate in 2.21 g of water was added. The reaction was stopped ...
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Abstract
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