Curable solid ink compositions
A technology of solid ink and composition, applied in the direction of ink, photosensitive materials for optomechanical equipment, instruments, etc., can solve the problems of crystalline wax usage restriction printing method, poor ink performance, poor light fastness, etc.
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[0113] Process A for the Preparation of Ethoxylated Octylphenol Derivative A ("Derivative A")
[0114] Add pre-melted 70g IGEPALCA210 (M W =261) and 80.0g Unilin 425 (OH#95.3, M W =589) mixture. The flask was placed in a 140°C oil bath with a thermometer, then heated and stirred. After approximately 5 minutes, 30 g of IPDI (MW=222) was added, followed by three drops of Fascat 4202 catalyst. An exotherm was observed. After about 1.5 hours, obtain the IR spectrum of reaction product, do not find isocyanate peak (about 2230em -1 ). Pour the contents into aluminum cans to cool and solidify.
[0115] Process B for the preparation of ethoxylated octylphenol derivatives B ("derivatives B")
[0116]Add pre-melted 29.9g IGEPALCA210 (OH#214.92, M W =261) and 67.9g Unilin 425 (OH#95.3, M W =589) mixture. The flask was placed in a 140°C oil bath with a thermometer and heated / stirred. After about 5 minutes, add 30g dicyclohexylmethane-4,4'-diisocyanate (H 12 MDI, M W = 262...
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