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Lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and use thereof

A technology of lycopene and emulsion, applied in the field of cigarettes, can solve the problems of poor stability of lycopene, difficult tobacco application, inconvenient production, etc., and achieve the effects of facilitating subsequent purification work, saving industrial production time, and saving usage.

Inactive Publication Date: 2013-01-23
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, since lycopene is an ester-soluble compound, it is insoluble in water, hardly soluble in methanol and ethanol, soluble in fat, oil, ether, petroleum ether, ethyl acetate, n-hexane and acetone, and easily soluble in benzene, chloroform and carbon disulfide. and other organic solvents, so its application in tobacco has certain difficulties. Patent CN200810048038.0 uses ethyl acetate and acetone to extract, and then makes it into the form of microcapsules, but because acetone is toxic, it is difficult to remove it. In addition, Microcapsules are solid, not easy to mix with other spices, which increases the difficulty of adding
CN200510056125.7 introduces emulsified lycopene and its preparation method, but it adopts high-speed shear emulsification, which is inconvenient to produce; CN200710119790.5 introduces the preparation method of transparent water-dispersed lycopene concentrate, which is lycopene Dissolved in edible oil and then emulsified, because the edible oil will have an adverse effect on the taste of cigarettes after being burned in cigarettes, it cannot be used in cigarettes, and the stability of lycopene is poor, and cigarettes need a long time How to improve the stability of lycopene is also a difficult problem in the prior art.

Method used

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  • Lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and use thereof
  • Lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and use thereof
  • Lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and use thereof

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Experimental program
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Effect test

Embodiment 1

[0036] Embodiment 1, the extraction of lycopene

[0037] 1. After adding 5% BHT to the tomato sample, beat it with a pulp masher, filter it to remove water initially, and process it twice at 60° C. with medical alcohol with a weight ratio of 1:3 (ketchup: ethanol). Each time for 1 hour, the tomato pomace was obtained by suction filtration.

[0038] 2. Then use the mixed solvent ethyl acetate-n-hexane (ratio of 3:1) as the extractant, the ratio of liquid to solid is 7:1 (solvent:tomato pomace; weight ratio), the extraction temperature is 40°C, and the extraction time is 0.5 hours.

[0039] 3. Concentrate the extract, cool it to room temperature, filter, and keep the precipitated crystals as lycopene;

[0040] Above-mentioned extract is characterized by infrared spectrophotometer (IR), and its spectrogram sees attached figure 1 ; The above-mentioned extract is characterized by high performance liquid chromatography (HPLC), and its spectrogram is shown in the attached image 3...

Embodiment 2

[0042] Embodiment 2: the preparation of lycopene emulsion

[0043] 1. Heat and dissolve 1 g of water, 10 g of ethylene glycol, 1.5 g of ethanol, and 10 g of sucrose fatty acid ester, and prepare the resulting mixture for later use;

[0044] 2. Dissolve 1g of lycopene, 15g of caryophyllene, and 0.02mg of BHT under heating and stirring at 120°C to obtain a lycopene mixture;

[0045]3. Then add dropwise the prepared mixed solution in step 1, dropwise or slowly add it to the lycopene mixed solution in step (2), and keep stirring. It is lycopene emulsion.

Embodiment 3

[0046] Embodiment 3: the preparation of lycopene emulsion

[0047] 1. Heat 5g of water, 5g of glycerin, 2.5g of ethanol, and 10g of glyceryl monostearate to dissolve, and the resulting mixture is ready for use;

[0048] 2. Heat and stir 0.08g lycopene, 2.5g caryophyllene, and 0.01mg BHT at 120°C to obtain a lycopene mixture;

[0049] 3. Then add dropwise the prepared mixed solution in step 1, dropwise or slowly add it to the lycopene mixed solution in step (2), and keep stirring. It is lycopene emulsion.

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Abstract

The invention discloses to a lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and a user thereof, belonging to the technical field of cigarettes. The lycopene emulsion of the invention is prepared by the following steps: [1], extracting the lycopene; and [2], preparing the lycopene emulsion, wherein the emulsion is one of sucrose fatty acid ester, glycerin monostearate, sorbitantristearate or polyoxyethylene sorbitan fatty acid ester (tween) or a mixture of any several substances. The assistant is one of propylene glycol, glycerine, ethylene glycol and ethanol or a mixture of any several substances. In the use of the lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes in cigarettes, the lycopene emulsion is independently matched with tobacco flavors for charging the tobacco leaves or flavoring the tobacco shreds. The lycopene emulsion disclosed by the invention is stable for at least 6 months. The cigarette with the lycopene emulsion is capable of effectively reducing the gas-phase free radicals of cigarettes by over 17%.

Description

technical field [0001] The invention belongs to the technical field of cigarettes, and in particular relates to an emulsified lycopene additive capable of reducing free radicals in the gas phase of cigarettes for adding material or flavoring to cigarettes, and its application in cigarettes. Background technique [0002] As we all know, smoking is harmful to health. Studies have shown that the main factors that cause smoking harm to the human body are: carcinogens in smoke such as polycyclic aromatic hydrocarbons (PHA), nitrosamines, etc., which can make cells cancerous; free radicals in smoke such as Hydroxyl free radicals (HO·), etc., are highly active and can damage human cells. In the past few decades, people have been devoting themselves to research on reducing the harm of smoking to human body. Such as CN200410022412.1, using bamboo leaf extract as a free radical scavenger for tobacco products, CN200410022439.0, using emblica extract as a free radical scavenger for tob...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/24A24B3/12
Inventor 刘鑫殷发强朱威何佳文熊国玺赵同林
Owner HUBEI CHINA TOBACCO IND
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