Lycopene emulsion capable of stably reducing gas-phase free radicals of cigarettes and use thereof
A technology of lycopene and emulsion, applied in the field of cigarettes, can solve the problems of poor stability of lycopene, difficult tobacco application, inconvenient production, etc., and achieve the effects of facilitating subsequent purification work, saving industrial production time, and saving usage.
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Embodiment 1
[0036] Embodiment 1, the extraction of lycopene
[0037] 1. After adding 5% BHT to the tomato sample, beat it with a pulp masher, filter it to remove water initially, and process it twice at 60° C. with medical alcohol with a weight ratio of 1:3 (ketchup: ethanol). Each time for 1 hour, the tomato pomace was obtained by suction filtration.
[0038] 2. Then use the mixed solvent ethyl acetate-n-hexane (ratio of 3:1) as the extractant, the ratio of liquid to solid is 7:1 (solvent:tomato pomace; weight ratio), the extraction temperature is 40°C, and the extraction time is 0.5 hours.
[0039] 3. Concentrate the extract, cool it to room temperature, filter, and keep the precipitated crystals as lycopene;
[0040] Above-mentioned extract is characterized by infrared spectrophotometer (IR), and its spectrogram sees attached figure 1 ; The above-mentioned extract is characterized by high performance liquid chromatography (HPLC), and its spectrogram is shown in the attached image 3...
Embodiment 2
[0042] Embodiment 2: the preparation of lycopene emulsion
[0043] 1. Heat and dissolve 1 g of water, 10 g of ethylene glycol, 1.5 g of ethanol, and 10 g of sucrose fatty acid ester, and prepare the resulting mixture for later use;
[0044] 2. Dissolve 1g of lycopene, 15g of caryophyllene, and 0.02mg of BHT under heating and stirring at 120°C to obtain a lycopene mixture;
[0045]3. Then add dropwise the prepared mixed solution in step 1, dropwise or slowly add it to the lycopene mixed solution in step (2), and keep stirring. It is lycopene emulsion.
Embodiment 3
[0046] Embodiment 3: the preparation of lycopene emulsion
[0047] 1. Heat 5g of water, 5g of glycerin, 2.5g of ethanol, and 10g of glyceryl monostearate to dissolve, and the resulting mixture is ready for use;
[0048] 2. Heat and stir 0.08g lycopene, 2.5g caryophyllene, and 0.01mg BHT at 120°C to obtain a lycopene mixture;
[0049] 3. Then add dropwise the prepared mixed solution in step 1, dropwise or slowly add it to the lycopene mixed solution in step (2), and keep stirring. It is lycopene emulsion.
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