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A mixing method for preparing diamond-reinforced metal matrix composites

A diamond reinforced and composite material technology, applied in the field of electronic packaging, can solve the problems of introducing impurities and reducing the thermal conductivity of diamond reinforced metal matrix composite materials.

Inactive Publication Date: 2011-12-14
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to solve the problem that ceramic materials such as zirconia and alumina are used as grinding balls in the mixing process of the existing diamond-reinforced metal matrix composite material, and impurities are introduced during the mixing process, resulting in the preparation of diamond-reinforced metal matrix composites. To solve the problem of lower thermal conductivity of composite materials, the invention provides a mixing method for preparing diamond-reinforced metal-matrix composite materials. The metal matrix material is used as the ball material, and the diamond-reinforced metal matrix prepared by wet ball milling is mixed. The thermal conductivity of matrix composites is significantly improved compared to existing methods

Method used

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Examples

Experimental program
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Effect test

specific Embodiment approach 1

[0012] Specific Embodiment 1: This embodiment is a mixing method for preparing diamond-reinforced metal matrix composites, which is achieved through the following steps: 1. Weigh the raw materials of diamond particles and metal matrix materials respectively, wherein the weight of the diamond particles weighed For the weight of the diamond in the designed diamond-reinforced metal matrix composite, the weight of the metal matrix material weighed is 93% to 97% of the weight of the metal matrix material in the designed diamond-reinforced metal matrix composite, and the metal matrix material is aluminum or copper; 2. Add the raw materials weighed in step 1 into the mixer, then add alcohol to the mixer, then add grinding balls, and carry out ball milling and mixing for 5-10 hours. Wherein, the volume ratio of alcohol to raw materials is not If it is lower than 3:1, the material of the grinding ball is a metal matrix material, and the mass ratio of the grinding ball to the metal matri...

specific Embodiment approach 2

[0018] Specific embodiment 2: The difference between this embodiment and specific embodiment 1 is that the diamond-reinforced metal matrix composite material designed in step 1 consists of 10% to 50% diamond and 50% to 90% metal matrix material by weight percentage composition. Other steps and parameters are the same as those in Embodiment 1.

specific Embodiment approach 3

[0019] Embodiment 3: The difference between this embodiment and Embodiment 1 is that the diamond-reinforced metal matrix composite material designed in Step 1 is composed of 30% diamond and 70% metal matrix material by weight percentage. Other steps and parameters are the same as those in Embodiment 1.

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Abstract

The invention provides a mixing method for preparation of a diamond enhanced metal matrix composite material and relates to a mixing mode in a process of preparing the diamond enhanced metal matrix composite material, and the method can be used for solving the problem that the thermal conductivity of the prepared diamond enhanced metal matrix composite material is reduced due to the fact that zirconia, alumina and other ceramic materials are adopted as grinding balls in the conventional preparation method of the diamond enhanced metal matrix composite material, and impurities are introduced in the mixing process. The mixing method comprises the following steps: firstly weighing diamond particles and a metal raw material, wherein the metal dosage accounts for 93-97% of the design dosage, the raw material is subjected to wet mixing and ball grinding by use of the grinding balls made of the metal raw material, and the metal matrix material is aluminum or copper. Impurities can be effectively prevented from being introduced by adopting the metal matrix material as the grinding ball material, so that the thermal conductivity of the prepared diamond enhanced metal matrix composite material is remarkably improved by over 39%.

Description

technical field [0001] The invention relates to a mixing method in the process of preparing a diamond-reinforced metal matrix composite material, in particular to a wet ball milling mixing method using metal matrix materials in the composite material as grinding balls, and belongs to the field of electronic packaging. Background technique [0002] Diamond / metal matrix composite material is a new type of thermal management material, and its advantages such as high thermal conductivity, low density and adjustable thermal expansion coefficient make it a hot research topic. The diamond-reinforced composite material prepared by powder metallurgy method has high density, which is the basis for obtaining high thermal conductivity. The powder metallurgy method involves the mixing process. The wet ball milling mixing method can obtain uniformly distributed particles. However, since most of the grinding balls currently used are ceramics such as zirconia and alumina, the metal matrix o...

Claims

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Application Information

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IPC IPC(8): C22C1/05C22C26/00
Inventor 朱嘉琦高明王永杰韩杰才
Owner HARBIN INST OF TECH