Anti-oxidant 168
An anti-oxidant, phosphorus trichloride technology, applied in the direction of organic chemistry, chemical instruments and methods, compounds of group 5/15 elements of the periodic table, etc., can solve the problems of endangering the health of workers, pollution, high cost, etc., and achieve the preparation Convenience, Pollution Reduction, and Harm Reduction Effects
Inactive Publication Date: 2012-06-06
天津市北方金恒新材料有限责任公司
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Problems solved by technology
Toxic substances that pollute the environment will be produced during the p
Method used
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Experimental program
Comparison scheme
Effect test
Embodiment 1
[0008] Example 1: An antioxidant 168 prepared by mixing 500Kg of 2,4-di-tert-butylphenol, 150Kg of phosphorus trichloride, and 5Kg of pyridine.
Embodiment 2
[0009] Example 2: An antioxidant 168 prepared by mixing 800Kg of 2,4-di-tert-butylphenol, 200Kg of phosphorus trichloride, and 10Kg of pyridine.
Embodiment 3
[0010] Example 3: An antioxidant 168 prepared by mixing 744Kg of 2,4-di-tert-butylphenol, 170Kg of phosphorus trichloride, and 8Kg of pyridine.
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Abstract
An anti-oxidant 168 is prepared from the following raw materials, by weight: 500-800 parts of 2,4-di-tert-butylphenol, 150-200 parts of phosphorus trichloride and 5-10 parts of pyridine. The invention has the following advantages and active effects: 1. reasonable formula and convenient preparation to increase production efficiency; 2. reduced pollution on the environment and reduced harm on workers; 3. an increased product yield higher than 90%; and 4. reduced production cost.
Description
Technical field: [0001] The invention relates to a production method of chemical products, in particular to a preparation method of antioxidant 168. Background technique: [0002] Antioxidant 168, chemical name tris(2,4-di-tert-butylphenyl) phosphite, molecular formula: C42H63O3P. Antioxidant 168 is an auxiliary antioxidant that is resistant to water extraction, low volatility, and high thermal stability. It can effectively decompose hydroperoxides generated during thermal processing of polymeric materials. As an auxiliary antioxidant, it is often used in combination with phenolic antioxidant 1010 or 1076 and has a synergistic effect. The product is widely used in polyolefins, styrene monomers and copolymers, elastomers, adhesives, engineering plastics (such as: polyester, polyurethane, PVC) and plasticizers, industrial fats, mineral oils and other organic substrates. [0003] The traditional synthesis method of antioxidant 168 has a yield of 88%, the yield of the final p...
Claims
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Patent Timeline

IPC IPC(8): C07F9/145
Inventor 索士满
Owner 天津市北方金恒新材料有限责任公司
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