Transparent ceramic white light emitting diode (LED) and preparation method thereof
A technology of transparent ceramics and LED chips, applied in the field of white light LEDs, can solve the problems of reduced luminous efficiency, poor heat dissipation performance, accelerated phosphor aging, etc., and achieve the effects of improving luminous performance, improving production efficiency, and improving heat dissipation effect.
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Embodiment 1
[0030] In this embodiment, the structure of the transparent ceramic white light LED is as follows figure 1 , figure 2As shown, it includes a support 1, a blue LED chip 2 and a cerium-doped yttrium aluminum garnet transparent ceramic sheet 3, the support is a circular frustum with grooves, and the cerium-doped yttrium aluminum garnet transparent ceramic sheet 3 is a circle with a thickness of 1 mm. sheet, with the chemical formula (Y 0.995 Ce 0.005 ) 3 al 5 o 12 The material is made, and the preparation method is as follows: according to the composition in the above chemical formula, Y(NO 3 ) 3 , NH 4 Al(SO 4 ) 2 , Ce(NO 3 ) 3 , set Y(NO 3 ) 3 , NH 4 Al(SO 4 ) 2 , Ce(NO 3 ) 3 Dissolve in deionized water and mix well to prepare Al 3+ A mixed salt solution with a concentration of 0.1mol / L. Will NH 4 HCO 3 Soluble in ethanol-water complex solvent to prepare NH 4 HCO 3 A precipitant solution with a concentration of 1mol / L, the volume ratio of ethanol to wat...
Embodiment 2
[0037] In this embodiment, the structure of the transparent ceramic white light LED is as follows figure 1 , figure 2 As shown, it includes a support 1, a blue LED chip 2 and a cerium-doped yttrium aluminum garnet transparent ceramic sheet 3, the support is a circular frustum with grooves, and the cerium-doped yttrium aluminum garnet transparent ceramic sheet 3 is a circle with a thickness of 1mm. sheet, with the chemical formula (Y 0.999 Ce 0.001 ) 3 al 5 o 12 The material is made, and the preparation method is as follows: according to the composition in the above chemical formula, Y(NO 3 ) 3 , NH 4 Al(SO 4 ) 2 , Ce(NO 3 ) 3 , set Y(NO 3 ) 3 , NH 4 Al(SO 4 ) 2 , Ce(NO 3 ) 3 Dissolve in deionized water and mix well to prepare Al 3+ A mixed salt solution with a concentration of 0.15mol / L. Will NH 4 HCO 3 Soluble in ethanol-water complex solvent to prepare NH 4 HCO 3 Concentration is the precipitant solution of 0.5mol / L, the volume ratio of described eth...
Embodiment 3
[0044] In this embodiment, the structure of the transparent ceramic white light LED is as follows figure 1 , figure 2 As shown, it includes a support 1, a blue LED chip 2 and a cerium-doped yttrium aluminum garnet transparent ceramic sheet 3, the support is a circular frustum with grooves, and the cerium-doped yttrium aluminum garnet transparent ceramic sheet 3 is a circle with a thickness of 1mm. sheet, with the chemical formula (Y 0.9995 Ce 0.0005 ) 3 al 5 o 12 The material is made, and the preparation method is as follows: according to the composition in the above chemical formula, Y(NO 3 ) 3 , Al(NO 3 ) 3 , Ce(NO 3 ) 3 , set Y(NO 3 ) 3 , Al(NO 3 ) 3 , Ce(NO 3 ) 3 Dissolve in deionized water and mix well to prepare Al 3+ A mixed salt solution with a concentration of 0.2mol / L. Will NH 4 HCO 3 Soluble in ethanol-water complex solvent to prepare NH 4 HCO 3 A precipitant solution with a concentration of 2mol / L, the volume ratio of ethanol to water is 1.2:...
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Abstract
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