Preparation method of pyrazolone/polymer composite photochromic film
A technology of pyrazolone and polymer is applied in the field of preparation of pyrazolone/polymer composite photochromic film, can solve problems such as inconvenience of manufacture, and achieve the effects of low cost, uniform texture and good transparency
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Embodiment 1
[0016] At room temperature, under the condition of magnetic stirring, slowly add 0.25 g of HPMC white powder into 20 ml of distilled water, and keep stirring to fully dissolve HPMC to form a clear solution. Then, under the condition of avoiding light, slowly add 0.05 g of DP3BrBP-PSC white powder into the clear solution, and continue to stir for 3 hours, so that DP3BrBP-PSC is well dispersed in the clear solution to obtain a co-suspension, After defoaming by standing in the dark, the blended suspension was slowly poured into a clean glass tank, and dried overnight at room temperature in the dark to obtain a pyrazolone / polymer composite photochromic film. The composite film has good photochromic properties, and it turns from white to yellow after being irradiated with 365nm ultraviolet light.
[0017] The above-mentioned composite film has good photochromic performance, and the ultraviolet absorption spectrum of the composite film is shown as follows: figure 1 As shown, it is ...
Embodiment 2
[0019] At 60°C, under the condition of magnetic stirring, slowly add 3 grams of PVA white particles into 20 ml of distilled water, and stir for 1 hour to fully dissolve the PVA and form a clear solution. Then, 0.06 g of DP3BrBP-PSC white powder was slowly added to the clear solution at room temperature and protected from light, and the stirring was continued for 5 hours, so that DP3BrBP-PSC was well dispersed in the clear solution to obtain a co-suspension, After defoaming by standing in the dark, the blended suspension was slowly poured into a clean glass tank, and dried overnight at room temperature in the dark to obtain a pyrazolone / polymer composite photochromic film. The composite film has good photochromic properties, and it turns from white to yellow after being irradiated with 365nm ultraviolet light.
[0020] After irradiating with 365nm ultraviolet light, the ultraviolet absorption spectrum of the composite film is as follows: image 3 As shown, it is found that a n...
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