Volatile oil for treating arthralgia and injuries of tendons and preparation method of volatile oil
A technology for volatile oil and arthralgia, which is applied in the field of volatile oil for treating arthralgia and tendon injury and its preparation, and achieves the effects of high extraction efficiency, convenient use, and anti-inflammatory and analgesic effects.
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Embodiment 1
[0033] Weigh the following raw materials in parts by weight: dried ginger 16g, Kaempfera 9g, Angelica dahurica 9g, Gansong 8g, Tangerine peel 9g, Angelica 4.5g, Clove 4.5g, Asarum 4g, Nepeta 4g, Guizhi 4g, Magnolia 3g, Rhizoma Chuanxiong 3g, 3g of cloves, 2g of herb, 2g of frankincense, 2g of myrrh, a total of 87g, and then crushed into 20-mesh powder, put the powder into the extraction kettle, and then put the CO 2 After passing through the booster system, it is sent to the extraction kettle and raw materials for CO 2 Supercritical extraction, control extraction pressure 20MPa, temperature 45°C, CO 2 With a flow rate of 20L / h and an extraction time of 1.5 hours, the CO dissolved in volatile oil 2 The fluid is transported to the separation tank, and the CO 2 Separation from volatile oil, the receiver collects volatile oil, CO 2 Recycle, get volatile oil 9.04g.
Embodiment 2
[0035] Weigh the following raw materials in parts by weight: 7g of dried ginger, 15g of kaempferen, 5g of Angelica dahurica, 12g of Gansong, 5g of tangerine peel, 9g of angelica, 3g of clove, 6g of asarum, 2g of nepeta, 6g of cassia twig, 2g of magnolia, 5g of chuanxiong, 2g of lovage, 3g of herb, 1g of frankincense, 3g of myrrh, 86g in total, and then crushed into 40-mesh powder, put the powder into the extraction kettle, and then put the CO 2 After passing through the booster system, it is sent to the extraction kettle and raw materials for CO 2 Supercritical extraction, control extraction pressure 35MPa, temperature 60°C, CO 2 With a flow rate of 20L / h and an extraction time of 2 hours, the CO dissolved in volatile oil 2 The fluid is transported to the separation tank, and the CO 2 Separation from volatile oil, the receiver collects volatile oil, CO 2 By recycling, 8.34g of volatile oil was obtained.
Embodiment 3
[0037] Weigh the following raw materials by weight, 18g of dried ginger, 5g of Kaempferen, 15g of Angelica dahurica, 4g of Gansong, 15g of tangerine peel, 3g of angelica, 9g of clove, 2g of asarum, 6g of nepeta, 2g of cassia twig, 5g of magnolia, 2g of chuanxiong, Duhuo 5g, Atractylodes 1g, Frankincense 3g, Myrrh 1g, a total of 96g, then crushed into 60-mesh powder, put the powder into the extraction kettle, and then put CO 2 After passing through the booster system, it is sent to the extraction kettle and raw materials for CO 2 Supercritical extraction, control extraction pressure 25MPa, temperature 50°C, CO 2 With a flow rate of 20L / h and an extraction time of 0.5 hours, the CO dissolved in volatile oil 2 The fluid is transported to the separation tank, and the CO 2 Separation from volatile oil, the receiver collects volatile oil, CO 2 Recycle, get volatile oil 9.27g.
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