Metallized surface of zirconia ceramic and preparation method

A zirconia ceramic and metallized surface technology, which is applied in the field of metallized surface and preparation of zirconia ceramics, can solve the problems of not meeting the air tightness requirements of devices and high connection strength, achieves good consistency, high bonding strength, and is suitable for strong effect

Inactive Publication Date: 2013-05-15
ZHEJIANG YATONG METAL CERAMICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology describes an improved method for producing highly pure ceramically colored surfaces that can be applied on various materials like ZrC or other oxides without losing their effectiveness over time due to factors like temperature changes (temperature affecting how well it works). These methods allow for precise adjustment of parameters during manufacturing processes while maintaining stability and reliance from each material' characteristics.

Problems solved by technology

This patents describes how strong connections may occur when connecting materials like zircite ceramic with steel without losing their effectiveness due to poor sealing performance caused by an oxidation process that occurs over time. Additionally, there exist methods for joining these components securely through physical contact instead of relying on adhesive bonds which could lose its ability if exposed to moisture. Therefore, researchers aiming to study better ways to connect ziriconcer ceramisms to iron substrates while maintaining sufficient air pressure within the joints themselves.

Method used

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  • Metallized surface of zirconia ceramic and preparation method

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Embodiment

[0032] The technological process of the present invention is as follows: each powder is mixed according to the weight ratio and ball milled → dried and sieved → stirred with binder → coated on the surface of zirconia ceramics (wet film thickness is about 30-100um) → protected in the atmosphere Next, metallization sintering→nickel plating→performance test of metallized products.

[0033] Describe in detail below by specific embodiment as follows:

[0034] 1. The selected powders are weighed according to the proportions in the table below, and placed in a 99% alumina ceramic ball mill tank, using anhydrous ethanol or butyl acetate as the medium, and using agate balls or alumina ceramic balls for grinding The balls are milled for more than 180 hours, taken out, placed in a stainless steel pan to dry, and passed through a 250-mesh sieve.

[0035] Table 1: Metallization formulation (weight percent)

[0036] Number and Composition

Mo

mn

SiO 2

CaO

75%...

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Abstract

The invention relates to a metallized surface of zirconia ceramic and a preparation method. The metallized surface of zirconia ceramic comprises of the following components by weight: 50-70% Mo powder, 11-19% of Mn powder, 6-14% of SiO2 powder, 0.2-2.5% of CaO, 5-15% of 75% alumina ceramic powder, 0-4% of ZrO2, and 0-5% of TiO2. Specifically, the 75% alumina ceramic powder is composed of the following components by weight: 73-79% of Al2O3, 11-17% of SiO2, 0-5% of BaO, 0.5-4% of CaO, and 0.5-2.5% of MgO. The preparation method includes: 1) conducting weighing and mixing according to the metallized formula proportion, placing the mixture in a high energy ball mill, carrying out high-energy ball milling for over 180h in an organic medium to prepare metallized powder; 2) adding a proper amount of an organic binder into the prepared metallized powder, fully stirring them, covering a cleaned zirconia ceramic surface with the mixture by means of silk screen printing, pad printing, spraying coating, pen coating or other modes, and performing natural drying or infrared ray drying; 3) sintering the metallized powder-covered zirconia ceramic under protection of a weak reducing atmosphere; and 4) subjecting the sintered product to nickel plating, thus obtaining a zirconia ceramic surface metallized product.

Description

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Claims

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Application Information

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Owner ZHEJIANG YATONG METAL CERAMICS
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