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Isobavachalcone microemulsion and preparation method thereof

A lipid chalcone microemulsion, isopsoralen chalcone technology, applied in the directions of botanical equipment and methods, biocides, disinfectants, etc., can solve the problem of high bacteriostatic activity, and achieve strong solubility and selectivity. Strong, formulation-stable effect

Active Publication Date: 2015-05-27
沈阳同祥生物农药有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen from Table 2 in the patent "Psoralen Chalcone Compounds and Psoralen Dihydroflavonoids Mixed Preparations for Plant Disease Prevention and Control" that the EC50 of isopsoralen chalcones on apple rot pathogens (to pathogen mycelium The inhibition rate of growth rate is 50% required concentration) is 4.51 mg / L, and the EC50 of psoralen dihydroflavone to apple rot bacteria is 8.62 mg / L. The EC50 of any kind of ratio of isopsoralenchalcone against apple rot pathogen is higher than 4.51 mg / L of isopsoralenchalcone single agent, and lower than 8.62 mg / L of psoralen dihydroflavone. L, indicating that the mixture of the two improves the activity of psoralen dihydroflavone, but neither has the high antibacterial activity of isopsoralen chalcone single agent

Method used

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  • Isobavachalcone microemulsion and preparation method thereof
  • Isobavachalcone microemulsion and preparation method thereof

Examples

Experimental program
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Effect test

example 1

[0022] Example 1: Preparation of 100g 0.1% isopsoralen chalcone microemulsion: Weigh 0.1g of pure isopsoralen chalcone, add n-methylpyrrolidone 10.4g, ethylene glycol 8.5g, stir until Completely dissolved, the isopsoralen chalcone solution is an oil phase; add 12g of emulsifier ZSL-64, 4g of calcium dodecylbenzenesulfonate to 65g of water in turn, and stir to form a transparent and uniform solution; finally, slowly drop the oil phase Put it into the solution, stir while adding dropwise, and observe the liquid state until a transparent and uniform solution is formed.

example 2

[0023] Example 2: Preparation of 100g 0.5% isopsoralen chalcone microemulsion: take by weighing 12.5g of psoraleae extract containing 4% isopsoralen chalcone, add n-methylpyrrolidone 12.5g, ethylene glycol Alcohol 5g, fully stirred until completely dissolved, the isopsoralen chalcone solution is an oil phase; emulsifier ZSL-64 10g, calcium dodecylbenzenesulfonate 1g were added to 59g water in sequence, and stirred to form a transparent homogeneous solution; Slowly drop the oil phase into the solution, stir while adding, observe the liquid state, until a transparent and uniform solution is formed.

example 3

[0024] Example 3: Preparation of 100g: 1% isopsoralen chalcone microemulsion: Weigh 1g of pure isopsoralen chalcone, add n-methylpyrrolidone 15g, ethylene glycol 4g, fully stir until completely dissolved , the isopsoralen chalcone solution is an oil phase; emulsifier ZSL-64 12.5g, calcium dodecylbenzenesulfonate 0.5g are added to 67g water in sequence, and stirred to form a transparent and uniform solution; finally, the oil phase is slowly dripped Put it into the solution, stir while adding dropwise, and observe the liquid state until a transparent and uniform solution is formed.

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PUM

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Abstract

An isopsoralen chalcone microemulsion and a preparation method thereof, relating to an agricultural fungicide and a preparation method thereof, comprising 0.1% to 10% of isopsoralen chalcone, 10% to 30% of a solvent and a co-solvent, The emulsifier is 12% to 20%, and the rest is water; first prepare the oil phase, mix the pure isopsoralen chalcone or the plant extract of isopsoralen chalcone with solvent and co-solvent, and stir until completely dissolved; Then prepare the water phase, add the emulsifier into the water and stir to form a transparent and uniform solution; finally, slowly drop the oil phase into the solution, stir while adding, and observe the liquid state until a transparent and uniform solution is formed. The preparation uses water instead of organic solvents, reducing environmental pollution. The microemulsion has better control effects on rice blast, apple rot, pepper anthracnose, cucumber gray mold and other plant fungal diseases and plant virus diseases. , in line with the quality standards of pesticide microemulsion products.

Description

technical field [0001] The invention relates to an agricultural fungicide and a preparation method thereof, in particular to an isopsoralen chalcone microemulsion and a preparation method thereof. Background technique [0002] Isopsoralen chalcone comes from the seeds of the leguminous plant Psoralen, which is a natural product. Moreover, isopsoralenchalcone has high inhibitory activity against important plant diseases such as rice blast fungus, tomato virus, apple rot fungus, and cucumber anthracnose fungus. Process this natural product into highly efficient, environmentally friendly, non-toxic, non-residual, less likely to produce drug resistance, relatively safe for humans and livestock, and can maintain high-quality agricultural products. Plant-derived biopesticides promote the sustainable development of agriculture. [0003] For this reason, the inventor has obtained the "Mixed Preparation of Psoralen Chalcone Compounds and Psoralen Dihydroflavonoids for Controlling ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N25/04A01N35/04A01P1/00A01P3/00
Inventor 关丽杰于海峰赵礼慧
Owner 沈阳同祥生物农药有限公司
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