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Extraction method for effective compositions of antrodia camphorata

An active ingredient, Antrodia camphorata technology, applied in the direction of producing fat, fat oil/fat production, etc., can solve the problems of flammable, explosive, unsafe, high extraction cost, and achieve the effect of high effective ingredients and easy operation

Inactive Publication Date: 2014-07-16
GUANGDONG MEDICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Extracting fats in the prior art is to use organic solvent extraction methods such as ether, and its main disadvantages are: 1. The extraction cost is high, and it is inflammable and explosive; 2. There are residual organic solvents in the extract, which affects people's life safety ; 3. Product yield is low

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Cleaning: Rinse Antrodia camphorata with pure water.

[0015] Vacuum freeze-drying: Antrodia camphorata is quick-frozen in a quick-freezer at -35°C to a central temperature of -18°C, dried at a vacuum of 90pa and a temperature of 42°C, and taken out when its water content is lower than 2%.

[0016] Pulverization: Use a frozen pulverizer to pulverize at a temperature of -26°C, and sieve at 30°C to obtain Antrodia camphorata powder.

[0017] Filling: Weigh 500g of Antrodia camphorata powder, put it into an extraction tank, seal it, close all valves, and check whether the temperature controller is in good condition.

[0018] Extraction tank: set the temperature of the extraction tank to 35°C, pressure: 25Mpa, CO 2 The flow rate is 35L / h, and food-grade 96% ethanol is added as an entrainer.

[0019] Separation tank: set the temperature of the separation tank to 30°C and the pressure to 10Mpa.

[0020] Refined column I: Set the temperature of refined column I to 25°C and ...

Embodiment 2

[0025] Cleaning: Rinse Antrodia camphorata with pure water.

[0026] Vacuum freeze-drying: Antrodia camphorata is quick-frozen in a quick-freezer at -36°C to a central temperature of -18°C, dried at a vacuum of 90pa and a temperature of 39°C, and taken out when its water content is lower than 2%.

[0027] Pulverization: Use a frozen pulverizer to pulverize at a temperature of -26°C, and sieve at 30°C to obtain Antrodia camphorata powder.

[0028] Filling: Weigh 500g of Antrodia camphorata powder, put it into an extraction tank, seal it, close all valves, and check whether the temperature controller is in good condition.

[0029] Extraction tank: Set the temperature of the extraction tank to 36°C, pressure: 28Mpa, CO 2 The flow rate is 36L / h, and food-grade 96% ethanol is added as an entrainer.

[0030] Separation tank: set the temperature of the separation tank to 32°C and the pressure to 11Mpa.

[0031] Refined column I: set the temperature of refined column I to 22°C and ...

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PUM

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Abstract

The invention relates to a method for extracting antrodia camphorata oil by employing a CO2 supercritical extraction process. The method comprises: cleaning antrodia camphorata, quickly freezing at -35 DEG C, drying in vacuum to have a water content less than 2%, crushing by a refrigeration pulverizer, sieving, and performing supercritical CO2 extraction; controlling an extraction tank to have the temperature of 35 DEG C and the pressure of 25 MPa, and controlling the CO2 flow to be 35 L / h, and adding food-grade 96% ethanol as an entrainer; controlling a separation tank to have the temperature of 30 DEG C and the pressure of 10 MPa; and controlling a rectification column to have the temperature of 25 DEG C and the pressure of 12 MPa, so as to obtain antrodia camphorata oil. The antrodia camphorata oil obtained by extraction has the advantages of high effective compositions, no residual organic solvents and the like, the extraction technology is easy to operate, the extraction yield is high, and the product can be used as a raw material for producing traditional Chinese medicines and health products.

Description

technical field [0001] The invention relates to an extraction method, in particular to an extraction method of active ingredients of Antrodia camphorata, belonging to the technical field of traditional Chinese medicine extraction. Background technique [0002] Antrodia cinnamomea, also known as camphor mushroom, is scientifically named Antrodia camphorata. It belongs to the order Aphylloides, Polyporaceae, and perennial fungi. It is a new fungus discovered by the biochemical community in 1990. Wild camphor wood has been listed as one of the national treasures by the government in recent years. The growth area of ​​Antrodia camphorata is in the mountains and forests at an altitude of 450-2000 meters in the mountains of Taiwan. Cinnamomum camphora wood wet surface, because of its high medicinal and edible value, and its output is scarce, the extraction research and application research of its active ingredients are beginning in China. [0003] Antrodia camphorata is rich in β...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/10C11B1/04
Inventor 刘立陆博
Owner GUANGDONG MEDICAL UNIV
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