Compositions containing kinase inhibitors
A kind of composition and medicine technology, applied in the field of treatment of diseases
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Embodiment 1
[0098] Example 1: N -(4-{4-amino-7-[1-(2-hydroxyethyl)-1 H -pyrazol-4-yl]thieno[3,2- c ]pyridin-3-yl}phenyl)- N Solubility of '-(3-fluorophenyl)urea free base in various media
[0099] Table 1:
[0100] Solvent / medium Solubility Water (in physiological pH range) < 30ng / mL
Embodiment 2
[0101] Example 2: Visual Inspection of Excipients at Different Cremophor EL / PEG-300 / Ethanol Ratio
[0102] Table 2:
[0103]
[0104] Mixtures containing PEG-300 and Cremophor EL resulted in cloudy excipients for dissolving the drug. Mixtures containing PEG-300, Cremophor EL, and ethanol resulted in clear, single-phase solutions only when PEG-300 and Cremophor EL were present in a 1:1 ratio. In other cases, mixtures containing PEG-300, Cremophor EL and ethanol also resulted in cloudy excipients.
Embodiment 3
[0105] Example 3: N -(4-{4-amino-7-[1-(2-hydroxyethyl)-1 H -pyrazol-4-yl]thieno[3,2- c ]pyridin-3-yl}phenyl)- N Solubility of '-(3-fluorophenyl)urea free base in PEG-300 / Cremophor EL / ethanol excipient
[0106] table 3:
[0107]
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