A coating anti-corrosion protective agent, its preparation method and application, and a hot-dip metal material
A technology of hot-dip metal and protective agent, which is applied in coatings, anti-corrosion coatings, polyester coatings, etc. It can solve the problems of poor corrosion resistance of protective films and achieve excellent storage resistance and corrosion resistance.
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[0013] The invention provides a preparation method of a coating anti-corrosion protective agent, which comprises mixing water, a silane coupling agent, a water-soluble silicate, a silicon oxide filler and a water-soluble film-forming resin in sequence; the silane coupling The agent includes a first silane coupling agent and a second silane coupling agent, and the first silane coupling agent is Cl(CH 2 ) 3 Si(OCH 3 ) 3 , Cl(CH 2 ) 3 Si(OC 2 h 5 ) 3 , Cl(CH 2 ) 3 SiCH 3 (OCH 3 ) 2 and Cl(CH 2 ) 3 SiCH 3 (OC 2 h 5 ) 2 At least one of; the second silane coupling agent is HS (CH 2 ) 3 Si(OCH 3 ) 3 、HS(CH 2 ) 3 Si(OC 2 h 5 ) 3 、HS(CH 2 ) 3 SiCH 3 (OCH 3 ) 2 and HS(CH 2 ) 3 SiCH 3 (OC 2 h 5 ) 2 at least one of the
[0014] Wherein, in detail, the method includes: (1) uniformly mixing water and the silane coupling agent to obtain a uniform liquid A; (2) uniformly mixing the uniform liquid A and a water-soluble silicate to obtain a uniform liquid ...
Embodiment 1
[0051] Mix 28 parts by weight of water and 1.6 parts by weight of silane coupling agent (composed of the first silane coupling agent and the second silane coupling agent) at a stirring speed of 1500 rpm to obtain uniform liquid A, Among them, the first silane coupling agent is Cl(CH 2 ) 3 Si(OCH 3 ) 3 , purchased from Hubei Debang Chemical New Material Co., Ltd., brand DB-231, the second silane coupling agent HS (CH 2 ) 3 Si(OCH 3 ) 3 , purchased from Hubei Debang Chemical New Material Co., Ltd., brand DB-590, the weight ratio of the first silane coupling agent and the second silane coupling agent is 1.5:1.
[0052] Mix all the uniform liquid A and 1 part by weight of water-soluble silicate (sodium metasilicate pentahydrate, purchased from Qingdao Darun Chemical Co., Ltd.) at a stirring speed of 1500 rpm until uniform to obtain uniform liquid B .
[0053] All the homogeneous liquid B and 0.72 parts by weight of silica filler (nano silica sol, purchased from Shandong Ba...
Embodiment 2
[0066] Mix 25 parts by weight of water and 1.4 parts by weight of silane coupling agent (composed of the first silane coupling agent and the second silane coupling agent) at a stirring speed of 1500 rpm to obtain a homogeneous liquid A, Among them, the first silane coupling agent is Cl(CH 2 ) 3 Si(OCH 3 ) 3 , purchased from Hubei Debang Chemical New Material Co., Ltd., brand DB-231, the second silane coupling agent is HS (CH 2 ) 3 Si(OC 2 h 5 ) 3 , purchased from Hubei Debang Chemical New Material Co., Ltd., brand DB-580, the weight ratio of the first silane coupling agent and the second silane coupling agent is 1.4:1.
[0067] All of the uniform liquid A and 1 part by weight of water-soluble silicate (potassium silicate, purchased from Baoding Runfeng Industrial Co., Ltd.) were mixed until uniform at a stirring speed of 1500 rpm to obtain a uniform liquid B.
[0068] Mix all the homogeneous liquid B and 0.6 parts by weight of silica filler (nano-silica sol, purchased ...
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