Method for environmentally preparing novel material capable of splitting chiral binaphthol from L-phenylalanine

Abstract

The invention relates to a method for environmentally preparing a novel material capable of splitting chiral binaphthol from L-phenylalanine. The method comprises the following steps: firstly, preparing N-methylacryloyl-L-phenylalanine methyl ester (A-L-M) in ionic liquid-1-ethyl-3-methylimidazole ethyl sulfate from L-phenylalanine; secondly, adding prepared A-L-M and a certain quantity of yttrium trifluoromethanesulfonate into ionic liquid-hexanolactam-tetrabutylammonium bromide, selecting and using a proper initiator, and obtaining a poly(A-L-M) material with a regular main chain in an inert atmosphere. According to the method, a preparation process is simple and good in repeatability, the used raw material-L-phenylalanine is wide in source and good in environmental compatibility, a reaction medium-ionic liquid is harmless to a human body and environment and can be recycled, and the prepared novel material is relatively high in yield, good in economic benefit and suitable for large-scale industrialized production.

Description

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AI Technical Summary

Benefits of technology

This patented technology uses certain types of compounds called polypyrrolidone or metaforminide acid dimers that have specific chemical structures attached at their ends. These specialized substances help break down bimolecular aggregates into smaller particles when mixed together during manufacturing processes. By mixing these small particles with other components like benzene, phenylenediaminetriphosphazoline, etc., they form larger composite products containing different parts such as bisbenzenesupportones, amino acids, carboxylic acids/esters, alcohols, olefins, alkenes, alkynes, oxoalkane rings, nitro groups, sulfur atoms, thiophenes, pyridines, pigments, dyes, metal chelators, enzyme cofactors, antioxidants, antiinflammatory agents, flavoring ingredients, and others involved in making plastic compositions.

Problems solved by technology

This patented technical problem addressed in this patents relating to improving the efficient manufacture of optical molecules like dichroism bifunctionals (DBFAs), including binaphornaes). Existing techniques involve complicated processes or use harmful environmental agents during purification steps leading to lower yields and increased costs associated with product isolations. Therefore, new ways to efficiently produce highly pure binaphthaquinone compositions without generating hazardous waste streams would improve both safety and commercial value.

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