Purification auxiliary material of microcrystalline graphite and production method thereof
A technology of microcrystalline graphite and pure auxiliary materials, applied in the field of microcrystalline graphite purification auxiliary materials and its production, can solve the problems of limited application range, low purification degree of purification auxiliary materials, etc., and achieve the effect of wide application range and simple formula
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Embodiment 1
[0016] A microcrystalline graphite purification auxiliary material is composed of the following ingredients in weight percentage: 40% of microcrystalline graphite, 20% of hydrochloric acid, 18% of phosphoric acid and 22% of ammonium fluoride. Among them, the concentration of hydrochloric acid is 36%, the density is 1.19; the concentration of phosphoric acid is 85%, the density is 1.69; the density of ammonium fluoride is 1.11.
[0017] A preparation method of microcrystalline graphite purification auxiliary materials, which comprises the following steps: (1) selecting microcrystalline graphite, hydrochloric acid, phosphoric acid and ammonium fluoride according to weight percentage; (2) sequentially mixing microcrystalline graphite with hydrochloric acid, phosphoric acid and fluorinated (3) Place the uniformly mixed mixture in an environment with a temperature of 60° C., dry the mixture, and cool to normal temperature to obtain the microcrystalline graphite purification auxiliar...
Embodiment 2
[0020] A microcrystalline graphite purification auxiliary material is composed of the following ingredients in weight percentage: 50% of microcrystalline graphite, 15% of hydrochloric acid, 12% of phosphoric acid, and 23% of ammonium fluoride. Among them, the concentration of hydrochloric acid is 36%, the density is 1.19; the concentration of phosphoric acid is 85%, the density is 1.69; the density of ammonium fluoride is 1.11.
[0021] The preparation method of the microcrystalline graphite purification auxiliary material comprises the following steps: (1) selecting microcrystalline graphite, hydrochloric acid, phosphoric acid and ammonium fluoride according to weight percentage; (2) sequentially mixing microcrystalline graphite with hydrochloric acid, phosphoric acid and ammonium fluoride Mixing; (3) placing the uniformly mixed mixture in an environment with a temperature of 70° C., drying the mixture, and cooling to normal temperature to obtain the microcrystalline graphite ...
Embodiment 3
[0024] A microcrystalline graphite purification auxiliary material is composed of the following ingredients in weight percentage: 45% of microcrystalline graphite, 25% of hydrochloric acid, 15% of phosphoric acid, and 15% of ammonium fluoride. Among them, the concentration of hydrochloric acid is 36%, the density is 1.19; the concentration of phosphoric acid is 85%, the density is 1.69; the density of ammonium fluoride is 1.11.
[0025] The preparation method of the microcrystalline graphite purification auxiliary material comprises the following steps: (1) selecting microcrystalline graphite, hydrochloric acid, phosphoric acid and ammonium fluoride according to weight percentage; (2) sequentially mixing microcrystalline graphite with hydrochloric acid, phosphoric acid and ammonium fluoride Mixing; (3) placing the uniformly mixed mixture in an environment with a temperature of 80° C., drying the mixture, and cooling to normal temperature to obtain the microcrystalline graphite ...
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