An internally heated high-pressure reactor

A high-pressure reactor and internal heating technology, applied to pressure vessels used in chemical processes, etc., can solve problems such as affecting the chemical reaction process and increasing costs

Inactive Publication Date: 2016-10-19
程维强 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Obtaining reaction information at different temperatures at the same time can only be done through multiple reactors, which will increase costs, and changes in reaction conditions will affect the chemical reaction process

Method used

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  • An internally heated high-pressure reactor

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Experimental program
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Effect test

Embodiment 1

[0028] Such as figure 1 As shown, an internally heated high-pressure reaction kettle includes a reaction tank composed of a reaction tank body 1 and a sealing cover 2. A single heat pipe 3 is inserted into the reaction tank from the sealing cover 2, and the diameter of the single heat pipe 3 is between 12mm- Between 15mm; single heat pipe 3 forms a temperature gradient area 4 from the center to the outer arm in the reaction tank; there is a partition 5 between the temperature gradient areas 4; there is an extension downward from the sealing cover 2 to each temperature gradient area 4 Quartz rod 7, the end of the quartz rod 7 outside the sealing cover 2 has an optical end face 12 for observation, through the optical end face 12, the reactor reaction changes in the temperature gradient area can be observed, and recorded according to the reaction time of the reactor. The reaction tank body 1 and the sealing cover 2 are sealed and connected by a flange.

Embodiment 2

[0030] Such as figure 1 As shown, an internally heated high-pressure reaction kettle includes a reaction tank composed of a reaction tank body 1 and a sealing cover 2. A single heat pipe 3 is inserted into the reaction tank from the sealing cover 2, and the diameter of the single heat pipe 3 is between 12mm- Between 15mm; single heat pipe 3 forms a temperature gradient area 4 from the center to the outer arm in the reaction tank; there is a partition 5 between the temperature gradient areas 4; there is an extension downward from the sealing cover 2 to each temperature gradient area 4 The quartz rod 7 of the quartz rod 7 outside the sealing cover 2 has an optical end face 12 for observation, and the reactor reaction change in the temperature gradient zone can be observed through the optical end face 12, and is recorded according to the reaction time of the reactor; 2. There is a stirring fork 6 extending downward toward each temperature gradient zone 4. The stirring fork 6 outs...

Embodiment 3

[0032] Such as figure 1 As shown, an internally heated high-pressure reaction kettle includes a reaction tank composed of a reaction tank body 1 and a sealing cover 2. A single heat pipe 3 is inserted into the reaction tank from the sealing cover 2, and the diameter of the single heat pipe 3 is between 12mm- Between 15mm; single heat pipe 3 forms a temperature gradient area 4 from the center to the outer arm in the reaction tank; there is a partition 5 between the temperature gradient areas 4; there is an extension downward from the sealing cover 2 to each temperature gradient area 4 The quartz rod 7 of the quartz rod 7 outside the sealing cover 2 has an optical end face 12 for observation, and the reactor reaction change in the temperature gradient zone can be observed through the optical end face 12, and is recorded according to the reaction time of the reactor; 2 There is a stirring fork 6 extending downward to each temperature gradient area 4, and the stirring fork 6 outsi...

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PUM

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Abstract

The invention relates to an internal-heating high-pressure reaction kettle. The internal-heating high-pressure reaction kettle comprises a reaction tank composed of a reaction tank body and a sealing cover; a single head heating pipe is arranged on the reaction tank body, and is extended into the reaction tank so as to form temperature gradient zones distributed from the center to the periphery in the reaction tank; separating plates are arranged among the temperature gradient zones; quartz rods are arranged on the sealing cover, and are extended downward into the temperature gradient zones; the ends of the quartz rods outside the sealing cover are provided with optical terminals used for observation; reaction change of the temperature gradient zones in the internal-heating high-pressure reaction kettle can be observed via the optical terminals, and recording is carried out based on reaction kettle reaction time; and the reaction tank body and the sealing cover are connected via flanges. Information of a same reaction under different temperatures can be obtained by using the internal-heating high-pressure reaction kettle without increasing equipment.

Description

technical field [0001] The invention relates to a reactor, in particular to an internally heated high-pressure reactor. Background technique [0002] Reactors are widely used in petroleum, chemical, rubber, pesticides, dyes, medicines, food, pressure vessels used to complete vulcanization, hydrogenation, alkylation, polymerization, condensation and other processes, such as reactors, reaction kettles, decomposition pots, polymerization kettle etc. The heating methods of the reactor include electric heating, hot water heating, heat transfer oil circulation heating, external (inner) coil heating, etc., and the cooling methods are jacket cooling and internal coil cooling. [0003] Regardless of the heating method used in the reactor, the chemical reaction process in the reactor is completed at a controlled temperature. Generally, the chemical reaction process is different at different temperatures, and in some cases the difference is quite large. of. [0004] Obtaining reacti...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J3/04
CPCB01J3/04
Inventor 程维强李进
Owner 程维强
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