Diagnostic kit and method for detecting V561D mutation of human PDGFRalpha gene
A technology of α gene and kit, which is applied in the field of diagnostic kits for detecting the V561D mutation of human PDGFRα gene, can solve the problems of high cost and unfavorable clinical detection, and achieve low cost, fast detection and good clinical application prospects
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Embodiment 1
[0039] Example 1 The present invention detects the kit and detection method of V561D mutation
[0040] PCR amplification reagent (50 servings):
[0041] components
1 serving
50 servings
MgCl2
5-10mmol
500mmol
dUTP PLUS
0.5μl
25μl
Various primers
0.1-1μl
50μl
Each probe
0.5-1.5μmol
75μmol
UNG
0.2μl
19μl
Taq
0.3μl
15μl
overall system
20μl
1000μl
[0042] Amplification primers and detection probes for PDGFRα gene V561D mutation:
[0043] Primers:
[0044] 12F 5'-tat gaa att cgc tgg agg ga-3' Forward (SEQ ID NO.1)
[0045] 12R 5'-AGTTGTGTGCAAGGGAAA-3' Reverse (SEQ ID NO.2)
[0046] Probe:
[0047] 12P FAM-5'-CCCATGGAACTTACCAAAGCACTAGTCC-3'-BQ1 Forward (SEQ ID NO.3)
[0048] Quality control primers and probes:
[0049] Primers:
[0050] 5'-cctcaagatcatcagcaatgcctc-3' Forward in CtlF (SEQ ID NO.4)
[0051] 5'-GTG GTC ATG AGT CCT TCC ACG ATA-3' Reve...
experiment example 1
[0102] Experimental example 1 The detection of the accuracy of kit and method of the present invention
[0103] 1. Sample to be tested
[0104] One clinical GIST paraffin tissue sample with known mutation type V561D and one known wild-type clinical GIST paraffin tissue sample were selected to detect human PDGFRα gene mutation results.
[0105] 2. Detection method
[0106] The method of the present invention: adopt the kit of embodiment 1, detect according to the method of embodiment 1.
[0107] Sample DNA extraction method: extract with Qiagen kit:
[0108] 1. Use a scalpel to remove the useless paraffin at the tissue border;
[0109] 2. Cut the paraffin-embedded tissue into 4 μm thick slices;
[0110] 3. Quickly use sterilized tweezers to take 2-6 pieces and put them into DNase / RNase Free EP tubes (each spreading area is 500 (maximum) mm) 2 , which is the size of a square with a side length of 1.6 cm;
[0111] 4. Add 800μl xylene, shake on the shaker for 10s, and centri...
experiment example 2
[0131] Experimental example 2 The specificity of kit and method of the present invention
[0132] 1. Sample to be tested
[0133] Randomly select 200 cases of clinical GIST paraffin tissue samples to detect human PDGFRα gene mutation results.
[0134] 2. Detection method
[0135] Sample DNA extraction method: extract with Qiagen kit:
[0136] ●Using a scalpel to remove useless paraffin at the tissue border;
[0137]●Slice the paraffin-embedded tissue into 4μm thick slices;
[0138] Quickly take 2-6 pieces with sterilized tweezers and put them into DNase / RNase Free EP tubes (the area of each sheet is 500 (maximum) mm) 2 , which is the size of a square with a side length of 1.6 cm;
[0139] ●Add 800μl xylene, shake on the shaker for 10s, and centrifuge at the maximum speed for 3 minutes;
[0140] ●Add 800μl xylene, shake on the shaker for 10s, and centrifuge at the maximum speed for 3 minutes;
[0141] Discard the xylene, add 800 μl absolute ethanol, and centrifuge at t...
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