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A kind of preparation method of titanium alloy dental implant surface composite coating

A technology of dental implants and surface compounding, which is used in implants, dentistry, prosthetics, etc., can solve the problems of low bonding strength of the interface between the coating and the titanium alloy matrix, complicated long-term maintenance of osseointegration, and shortened service life. To achieve the effect of improving hydrophilic properties and cell adhesion, good long-term biosafety and stability, and increasing surface energy

Active Publication Date: 2017-06-06
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although people have used a variety of surface engineering methods to improve the comprehensive performance of medical titanium alloy materials and have made a lot of work and made gratifying progress, the low interface bonding strength between the coating and the titanium alloy substrate still plagues this type of technology. Bottlenecks in clinical application
In addition, under the joint action of the mechanical environment and the erosion of biological fluids, the coating of orthopedic implants is easy to fall off and dissolve, resulting in a decrease in the biological activity of the material and a shortened service life.
An additional challenge is the presence of an additional interface between the coating and the substrate, complicating long-term maintenance of osseointegration

Method used

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  • A kind of preparation method of titanium alloy dental implant surface composite coating

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] This embodiment includes the following steps:

[0027] Step 1. Perform sandblasting on the surface of the titanium alloy dental implant to be treated, and then perform ultrasonic cleaning and vacuum drying on the titanium alloy dental implant after the sandblasting treatment; the titanium alloy is Ti-6Al-4V titanium alloy, and the The sandblasting pressure of the sandblasting treatment is 0.6MPa, the sandblasting angle is 50 °, the sandblasting distance is 2cm, and the sandblasting time is 40s. The sand grains used in the sand blasting process are white corundum sand, and the grain size of the sand grains is 38 μm to 65 μm; the specific process of ultrasonic cleaning is as follows: first, ultrasonically clean the titanium alloy dental implant after sandblasting with deionized water for 10 minutes, then use acetone to ultrasonically clean for 10 minutes, and then use absolute ethanol to ultrasonically clean for 10 minutes;

[0028] Step 2. Immerse the vacuum-dried titani...

Embodiment 2

[0033] This embodiment includes the following steps:

[0034] Step 1. Perform sandblasting on the surface of the titanium alloy dental implant to be treated, and then perform ultrasonic cleaning and vacuum drying on the titanium alloy dental implant after the sandblasting treatment; the titanium alloy is a Ti-6Al-7Nb titanium alloy, and the The sandblasting pressure of the sandblasting treatment is 1.0MPa, the sandblasting angle is 50°, the sandblasting distance is 2cm, and the sandblasting time is 120s. The sand grains used in the sand blasting treatment are brown corundum, and the grain size of the sand grains is 65 μm. ~104 μm; the specific process of ultrasonic cleaning is as follows: first, ultrasonically clean the titanium alloy dental implant after sandblasting with deionized water for 5 minutes, then use acetone to ultrasonically clean for 5 minutes, and then use absolute ethanol to ultrasonically clean for 5 minutes;

[0035] Step 2. Immerse the vacuum-dried titanium ...

Embodiment 3

[0040] This embodiment includes the following steps:

[0041] Step 1. Perform sandblasting on the surface of the titanium alloy dental implant to be treated, and then perform ultrasonic cleaning and vacuum drying on the titanium alloy dental implant after the sandblasting treatment; the titanium alloy is Ti-3Zr-2Sn-3Mo-25Nb Titanium alloy, the sandblasting pressure of the sandblasting treatment is 1.0MPa, the sandblasting angle is 85 °, the sandblasting distance is 4cm, and the sandblasting time is 120s. The sand grains used in the sand blasting process are silica sand, and the sand grains The particle size is 38 μm to 104 μm; the specific process of ultrasonic cleaning is as follows: first, ultrasonically clean the titanium alloy dental implant after sandblasting for 15 minutes with deionized water, then ultrasonically clean it with acetone for 15 minutes, and then use absolute ethanol to ultrasonically clean it for 15 minutes ;

[0042] Step 2. Immerse the vacuum-dried tita...

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Abstract

The invention discloses a preparation method of a composite coating on the surface of a titanium alloy dental implant. The preparation method comprises the following steps that firstly, the surface of the titanium alloy dental implant is subjected to sand blasting, ultrasonic cleaning and then vacuum drying; secondly, the titanium alloy dental implant is subjected to acid etching processing, ultrasonic cleaning and then vacuum drying; thirdly, nitrogen is utilized for blowing the titanium alloy dental implant, and then electrochemical dealloying treatment is conducted; and fourthly, the titanium alloy dental implant is subjected to ultrasonic washing and vacuum drying, and then the composite coating is generated on the surface of the titanium alloy dental implant. The sand blasting, acid etching processing and electrochemical dealloying treatment technological processes are combined, so that the composite coating with micro-voids distributed in a graded mode is formed on the surface of the titanium alloy dental implant; the surface micro-voids can accelerate bone healing after the titanium alloy dental implant is implanted into a human body; the bone integration performance of the titanium alloy dental implant and the bone tissue is improved; the long-term stability and service performance are greatly improved after the titanium alloy dental implant is implanted into the human body.

Description

technical field [0001] The invention belongs to the technical field of surface modification of oral titanium alloy dental implants, and in particular relates to a method for preparing a composite coating on the surface of titanium alloy dental implants. Background technique [0002] Modern oral implant technology originated in the 1930s. In the mid-1950s, Professors Branemark and Albrektsson of the University of Gothenburg in Sweden used high-purity titanium as the implant material in the study of microvascular blood flow in the bone marrow cavity. Long-term observations have been made on titanium materials that have been injected into animals, and it is found that pure titanium has good biocompatibility with the body, and pure titanium has an unusually strong bond with the tibia of rabbits. Professor Branemark proposed the concept of osseointegration, which refers to a direct and firm combination between the load-bearing implant and the living bone tissue. The theory of os...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C25F3/08C25F3/14C23F1/26A61C8/00
Inventor 余森于振涛牛金龙刘春潮韩建业张亚峰刘汉源刘少辉
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH